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McCampbell Analytical, Inc. <br />"When Quality Counts" <br />1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 <br />http://www.mccampbell.com / main@mccampbell.com <br /> <br />Quality Control Report <br />Client: Yara North America WorkOrder: 2101638 <br />Date Prepared: 01/14/2021 BatchID: 213160 <br />Date Analyzed: 01/14/2021 <br /> <br />Extraction Method: SW5030B <br />Instrument: GC45 <br /> <br />Analytical Method: SW8260B <br />Matrix: Soil Unit: mg/kg <br />Project: New Site Pond <br /> <br />Sample ID: MB/LCS/LCSD-213160 <br />QC Summary Report for SW8260B <br />Analyte LCS <br />Result <br />LCSD <br />Result <br />SPK <br />Val <br />LCS <br />%REG <br />LCSD <br />%REG <br />LCS/LCSD <br />Limits <br />RPD RPD <br />Limit <br />cis-1,3-Dichloropropene 0.0190 0.0180 0.020 95 90 60-140 5.45 20 <br />trans-1,3-Dichloropropene 0.0192 0.0181 0.020 96 90 60-140 5.86 20 <br />Diisopropyl ether (DIPE) 0.0174 0.0163 0.020 87 82 60-140 6.55 20 <br />Ethylbenzene 0.0203 0.0192 0.020 101 96 60-140 5.62 20 <br />Ethyl tert-butyl ether (ETBE) 0.0173 0.0162 0.020 87 81 60-140 6.43 20 <br />Freon 113 0.0142 0.0132 0.020 71 66 50-140 7.09 20 <br />Hexachlorobutadiene 0.0230 0.0214 0.020 115 107 60-140 7.46 20 <br />Hexachloroethane 0.0183 0.0171 0.020 92 86 60-140 6.97 20 <br />2-Hexanone 0.0143 0.0131 0.020 71 65 40-140 8.54 20 <br />lsopropylbenzene 0.0236 0.0218 0.020 118 109 60-140 7.89 20 <br />4-Isopropyl toluene 0.0242 0.0224 0.020 121 112 60-150 7.74 20 <br />Methyl-t-butyl ether (MTBE) 0.0169 0.0160 0.020 85 80 50-140 5.96 20 <br />Methylene chloride 0.0176 0.0165 0.020 88 82 60-140 6.51 20 <br />4-Methyl-2-pentanone (MIBK) 0.0173 0.0157 0.020 87 79 50-140 9.43 20 <br />Naphthalene 0.00988 0.00821 0.020 49,F2 41,F2 50-140 18.5 20 <br />n-Propyl benzene 0.0232 0.0215 0.020 116 107 60-140 7.63 20 <br />Styrene 0.0182 0.0173 0.020 91 86 60-140 5.23 20 <br />1,1,1,2-Tetrachloroethane 0.0172 0.0163 0.020 86 81 60-140 5.78 20 <br />1,1,2,2-Tetrachloroethane 0.0184 0.0168 0.020 92 84 40-140 9.20 20 <br />Tetrachloroethene 0.0189 0.0179 0.020 94 89 60-140 5.43 20 <br />Toluene 0.0210 0.0194 0.020 105 97 60-140 7.90 20 <br />1,2,3-Trichlorobenzene 0.0129 0.0112 0.020 64 56 40-140 13.5 20 <br />1,2,4-Trichlorobenzene 0.0161 0.0148 0.020 81 74 50-140 8.66 20 <br />1,1,1-Trichloroethane 0.0169 0.0159 0.020 84 79 60-140 5.86 20 <br />1,1,2-Trichloroethane 0.0174 0.0161 0.020 87 81 60-140 7.53 20 <br />Trichloroethene 0.0171 0.0162 0.020 86 81 60-140 5.59 20 <br />Trichlorofluoromethane 0.0149 0.0135 0.020 74 67 50-140 9.88 20 <br />1,2,3-Trichloropropane 0.00888 0.00806 0.010 89 81 40-140 9.73 20 <br />1,2,4-Trimethylbenzene 0.0230 0.0212 0.020 115 106 30-140 7.89 20 <br />1,3,5-Trimethylbenzene 0.0230 0.0215 0.020 115 107 60-140 6.60 20 <br />Vinyl Chloride 0.00622 0.00584 0.010 62 58 30-140 6.33 20 <br />m,p-Xylene 0.0404 0.0383 0.040 101 96 60-140 5.29 20 <br />o-Xylene 0.0191 0.0182 0.020 95 91 60-140 4.62 20 <br />(Cont.) <br />CA ELAP 1644 • NELAP 40330RELAP <br />Page 37 of 51