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cp McCampbell Analytical, Inc. <br />"When Quality Counts" <br />1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 <br />http://www.mccampbell.com/ E-mail: tnain@rnccampbell.com <br /> <br />Quality Control Report <br />Client: Yara North America <br />Date Prepared: 01/15/2021 <br />Date Analyzed: 01/15/2021 <br />Instrument: GC48 <br />Matrix: Soil <br />Project: New Site Pond <br />WorkOrder: 2101638 <br />BatchID: 213244 <br />Extraction Method: 5W3550B <br />Analytical Method: 5W8270C <br />Unit: mg/Kg <br />Sample ID: MB/LCS/LCSD-213244 <br />QC Summary Report for SW8270C <br />Analyte LCS <br />Result <br />LCSD <br />Result <br />SPK <br />Val <br />LCS <br />%REC <br />LCSD <br />%REC <br />LCS/LCSD <br />Limits <br />RPD RPD <br />Limit <br />Benzo (g,h,i) perylene 0.0464 0.0468 0.062 74 75 70-130 0.683 30 <br />Benzo (k) fluoranthene 0.0574 0.0545 0.062 92 87 70-130 5.10 30 <br />Benzyl Alcohol 3.85 3.41 6.25 62,F2 55,F2 70-130 12.2 30 <br />Bis (2-chloroethoxy) Methane 1.11 1.04 1.25 88 84 70-130 5.77 30 <br />Bis (2-chloroethyl) Ether 0.0591 0.0579 0.062 95 93 60-130 1.95 30 <br />Bis (2-chloroisopropyl) Ether 0.0693 0.0654 0.062 111 105 60-130 5.77 30 <br />Bis (2-ethylhexyl) Adipate 1.22 1.16 1.25 98 93 60-130 5.24 30 <br />Bis (2-ethylhexyl) Phthalate 0.0461 0.0449 0.062 74 72 60-130 2.45 30 <br />Butylbenzyl Phthalate 0.0549 0.0526 0.062 88 84 60-130 4.35 30 <br />Chrysene 0.0557 0.0565 0.062 89 90 70-130 1.41 30 <br />Dibenzo (a,h) anthracene 0.0441 0.0439 0.062 70 70 70-130 0.410 30 <br />Dibenzofuran 1.06 1.07 1.25 85 86 60-130 1.01 30 <br />Diethyl Phthalate 0.0504 0.0504 0.062 81 81 70-130 0.0772 30 <br />Dimethyl Phthalate 0.0500 0.0503 0.062 80 81 70-130 0.704 30 <br />Di-n-butyl Phthalate 0.0453 0.0444 0.062 72 71 60-130 1.95 30 <br />Di-n-octyl Phthalate 0.0351 0.0339 0.062 56,F2 54,F2 60-130 3.39 30 <br />Fluoranthene 0.0465 0.0454 0.062 74 73 70-130 2.36 30 <br />Fluorene 0.0611 0.0616 0.062 98 98 60-130 0.703 30 <br />Hexachlorobenzene 0.0510 0.0494 0.062 82 79 70-130 3.06 30 <br />Hexachlorobutadiene 0.0528 0.0518 0.062 84 83 70-130 1.91 30 <br />Hexachlorocyclopentadiene 4.14 4.16 6.25 66 67 60-130 0.360 30 <br />Hexachloroethane 0.0541 0.0531 0.062 87 85 70-130 1.90 30 <br />Indeno (1,2,3-cd) pyrene 0.0467 0.0467 0.062 75 75 70-130 0.00932 30 <br />Isophorone 1.01 0.996 1.25 81 80 60-130 1.35 30 <br />Naphthalene 0.0500 0.0487 0.062 80 78 70-130 2.58 30 <br />Nitrobenzene 1.12 1.13 1.25 89 91 60-130 1.50 30 <br />N-Nitrosodimethylamine 5.77 5.78 6.25 92 92 70-130 0.0156 30 <br />N-Nitrosodi-n-propylamine 1.02 1.02 1.25 82 82 60-130 0.365 30 <br />N-Nitrosodiphenylamine 1.03 1.01 1.25 83 80 70-130 2.68 30 <br />Pentachlorophenol 0.213 0.207 0.31 68 66 50-130 2.66 30 <br />Phenanthrene 0.0504 0.0494 0.062 81 79 60-130 1.85 30 <br />Phenol 0.247 0.240 0.25 99 96 60-130 2.97 30 <br />Pyrene 0.0608 0.0592 0.062 97 95 70-130 2.65 30 <br />Pyridine 1.08 1.05 1.25 87 84 60-130 3.02 30 <br />(Cont.) <br />CA ELAP 1644 • NELAP 40330RELAP <br />Page 43 of 51