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March 16, 2022 Lab ID : STK2232777 <br />San Joaquin Co. Environmental Health Dep Customer :3-17919 <br />Quality Control - Inorganic <br />Constituent <br />Method <br />Date/ID <br />Type <br />Units <br />Conc. <br />QC Data <br />DQO <br />Note <br />Wet Chem <br />Nitrite <br />300.0 <br />(STK2232777-001) <br />MSD <br />mg/L <br />30.00 <br />99.7% <br />74-126 <br />MSRPD <br />mg/L <br />10.00 <br />3.4% <br /><20 <br />300.0 <br />03/03/22:203334njb <br />ICB <br />mg/l <br />0.00 <br />0.5 <br />ICV <br />mg/I <br />15.00 <br />102% <br />90-110 <br />CCB <br />mg/1 <br />0.00 <br />0.5 <br />CCV <br />mg/I <br />15.00 <br />103% <br />90-110 <br />Nitrite Nitrogen <br />300.0 <br />03/03/22:202428NJB <br />Blank <br />mg/L <br />ND <br /><0.2 <br />Sulfate <br />300.0 <br />03/03/22:202428NJB <br />Blank <br />mg/L <br />ND <br /><0.5 <br />LCS <br />mg/L <br />50.00 <br />99.9% <br />90-110 <br />MS <br />mg/L <br />100.0 <br />94.2% <br />82-124 <br />(STK2232691-001) <br />MSD <br />mg/L <br />100.0 <br />102% <br />82-124 <br />MSRPD <br />mg/L <br />10.00 <br />7.8% <br /><23 <br />MS <br />mg/L <br />100.0 <br />94.0% <br />82-124 <br />(STK2232777-001) <br />MSD <br />mg/L <br />100.0 <br />97.1 % <br />82-124 <br />MSRPD <br />mg/L <br />10.00 <br />1 3.1% <br /><23 <br />300.0 <br />03/03/22:203334njb <br />ICB <br />mg/I <br />0.165 <br />0.5 <br />ICV <br />mg/I <br />50.00 <br />102% <br />90-110 <br />CCB <br />mg/l <br />0.167 <br />0.5 <br />CCV <br />mg/I <br />50.00 <br />102% <br />90-110 <br />Nitrate + Nitrite as N <br />450ONO3F <br />03/01/22:202359vvh <br />Blank <br />mg/L <br />ND <br /><0.2 <br />LCs <br />mg/L <br />11.22 <br />98.3% <br />80-120 <br />MS <br />mg/L <br />5.609 <br />97.7% <br />5-285 <br />(STK2232783-001) <br />MSD <br />mg/L <br />5.609 <br />101% <br />5-285 <br />MSRPD <br />I mg/L <br />5.609 <br />1.9% <br />1 <30.4 <br />450ONO3F <br />03/01/22:203099vvh <br />ICB <br />mg/I <br />0.0730 <br />0.2 <br />ICV <br />mg/I <br />11.22 <br />97.9% <br />90-110 <br />CCB <br />mg/I <br />0.0480 <br />0.2 <br />CCV <br />mg/I <br />11.22 <br />97.3% <br />90-110 <br />Nitrate as NO3 <br />450ONO3F <br />03/01/22:202359vvh <br />Blank <br />mg/L <br />ND <br /><0.9 <br />Nitrate Nitrogen <br />450ONO3F <br />03/01/22:202359vvh <br />Blank <br />mg/l, <br />ND <br /><0.2 <br />MBAs <br />5540C <br />02/26/22:202974amm <br />CCB <br />mg/I <br />-0.0524 <br />0.25 <br />CCV <br />mg/l <br />1.000 <br />102% <br />90-110 <br />CCB <br />mg/l <br />-0.0568 <br />0.25 <br />CCV I <br />mg/I <br />1.000 <br />99.4% <br />90-110 <br />MBAs Extraction <br />5540C <br />02/26/22:202291amm <br />Blank <br />mg/L <br />ND <br /><0.1 <br />LCS <br />mg/L <br />0.5000 <br />105% <br />86-114 <br />BS <br />mg/L <br />0.5000 <br />101% <br />86-114 <br />BSD <br />mg/L <br />0.5000 <br />99.3% <br />86-114 <br />BSRPD <br />mg/L <br />0.5000 1 <br />1.8% <br /><5 <br />Definition <br />ICV : Initial Calibration Verification - Analyzed to verify the instrument calibration is within criteria. <br />ICB : Initial Calibration Blank - Analyzed to verify the instrument baseline is within criteria. <br />CCV : Continuing Calibration Verification - Analyzed to verify the instrument calibration is within criteria. <br />CCB : Continuing Calibration Blank - Analyzed to verify the instrument baseline is within criteria. <br />Blank : Method Blank - Prepared to verify that the preparation process is not contributing contamination to the samples. <br />LCS : Laboratory Control Standard/Sample - Prepared to verify that the preparation process is not affecting analyte recovery. <br />MS Matrix Spikes - A random sample is spiked with a known amount of analyte. The recoveries are an indication of how that sample <br />matrix affects analyte recovery. <br />MSD : Matrix Spike Duplicate of MS/MSD pair - A random sample duplicate is spiked with a known amount of analyte. The recoveries <br />are an indication of how that sample matrix affects analyte recovery. <br />BS : Blank Spikes - A blank is spiked with a known amount of analyte. It is prepared to verify that the preparation process is not <br />affecting analyte recovery. <br />BSD : Blank Spike Duplicate of BS/BSD pair - A blank duplicate is spiked with a known amount of analyte. It is prepared to verify that <br />the preparation process is not affecting analyte recovery. <br />Page 8 of 9 <br />