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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11426-002-SA Date Extracted: 04-19-2018 ICal: PCDDFAL3-12-22-17 Acquired: 04-21-2018
<br />Client ID: SP2-2 Date Received: 04-05-2018 GC Column: DB5MS 2005 WHO TEQ: 4.65
<br />Matrix: Solid Amount: 5.00 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4479 % Solids: 95.91
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.176 - 0.0315
<br />1,2,3,7,8-PeCDD 0.494 - J 0.494 0.0468
<br />1,2,3,4,7,8-HxCDD 1.03 - J 0.103 0.0503
<br />1,2,3,6,7,8-HxCDD 4.52 - J 0.452 0.0490 Total TCDD 0.836 -J
<br />1,2,3,7,8,9-HxCDD 2.42 - J 0.242 0.0488 Total PeCDD 5.77 -M
<br />1,2,3,4,6,7,8-HpCDD 123 -1.23 0.0541 Total HxCDD 35.3 -
<br />OCDD 1110 -0.333 0.0888 Total HpCDD 236 -
<br />2,3,7,8-TCDF 2.17 - F 0.217 0.0243
<br />1,2,3,7,8-PeCDF 0.818 - J 0.0245 0.0285
<br />2,3,4,7,8-PeCDF 1.38 - J 0.414 0.0298
<br />1,2,3,4,7,8-HxCDF 2.55 - J 0.255 0.0255
<br />1,2,3,6,7,8-HxCDF 3.14 - J 0.314 0.0253
<br />2,3,4,6,7,8-HxCDF 1.76 - J 0.176 0.0279
<br />1,2,3,7,8,9-HxCDF 1.01 - J 0.101 0.0367 Total TCDF 17.3 -
<br />1,2,3,4,6,7,8-HpCDF 24.3 -0.243 0.0321 Total PeCDF 12.6 -
<br />1,2,3,4,7,8,9-HpCDF 4.09 - J 0.0409 0.0396 Total HxCDF 22.7 -
<br />OCDF 51.3 -0.0154 0.0843 Total HpCDF 54.6 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 102 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 86.0 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 95.4 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 81.5 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 73.0 23.0 - 140
<br />13C-OCDD 60.3 17.0 - 157
<br />13C-2,3,7,8-TCDF 102 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 83.0 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 81.9 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 82.1 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 83.4 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 84.9 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 83.6 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 72.3 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 82.3 26.0 - 138
<br />13C-OCDF 60.6 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 94.4 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/25/2018
<br />5172 Hillsdale Circle * El Dorado Hills, CA 95762 * Tel (916) 934-0900 * Fax (916) 934-0999 * www.frontieranalytical.com
<br />4/26/2018
<br />of 000020000006
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