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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11426-004-SA Date Extracted: 04-19-2018 ICal: PCDDFAL3-12-22-17 Acquired: 04-21-2018
<br />Client ID: SP2-4 Date Received: 04-05-2018 GC Column: DB5MS 2005 WHO TEQ: 2.96
<br />Matrix: Solid Amount: 5.04 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4479 % Solids: 92.56
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.191 - 0.0315
<br />1,2,3,7,8-PeCDD 0.588 - J 0.588 0.0468
<br />1,2,3,4,7,8-HxCDD 0.810 - J 0.0810 0.0503
<br />1,2,3,6,7,8-HxCDD 2.24 - J 0.224 0.0490 Total TCDD 0.388 -J
<br />1,2,3,7,8,9-HxCDD 1.42 - J 0.142 0.0488 Total PeCDD 3.70 -J,M
<br />1,2,3,4,6,7,8-HpCDD 56.2 -0.562 0.0541 Total HxCDD 18.2 -
<br />OCDD 495 -0.149 0.0888 Total HpCDD 105 -
<br />2,3,7,8-TCDF 1.93 -0.193 0.0243
<br />1,2,3,7,8-PeCDF 0.497 - J 0.0149 0.0285
<br />2,3,4,7,8-PeCDF 1.33 - J 0.399 0.0298
<br />1,2,3,4,7,8-HxCDF 1.65 - J 0.165 0.0255
<br />1,2,3,6,7,8-HxCDF 1.20 - J 0.120 0.0253
<br />2,3,4,6,7,8-HxCDF 0.978 - J 0.0978 0.0279
<br />1,2,3,7,8,9-HxCDF 0.563 - J 0.0563 0.0367 Total TCDF 12.4 -M
<br />1,2,3,4,6,7,8-HpCDF 13.6 -0.136 0.0321 Total PeCDF 10.8 -
<br />1,2,3,4,7,8,9-HpCDF 1.58 - J 0.0158 0.0396 Total HxCDF 16.5 -
<br />OCDF 40.7 -0.0122 0.0843 Total HpCDF 38.4 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 101 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 96.8 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 91.3 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 92.4 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 79.7 23.0 - 140
<br />13C-OCDD 67.8 17.0 - 157
<br />13C-2,3,7,8-TCDF 101 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 89.6 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 87.4 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 95.0 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 98.5 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 93.7 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 94.1 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 80.8 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 87.1 26.0 - 138
<br />13C-OCDF 69.5 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 94.1 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/25/2018
<br />5172 Hillsdale Circle * El Dorado Hills, CA 95762 * Tel (916) 934-0900 * Fax (916) 934-0999 * www.frontieranalytical.com
<br />4/26/2018
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