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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11426-006-SA Date Extracted: 04-19-2018 ICal: PCDDFAL3-12-22-17 Acquired: 04-21-2018
<br />Client ID: SP2-6 Date Received: 04-05-2018 GC Column: DB5MS 2005 WHO TEQ: 2.71
<br />Matrix: Solid Amount: 5.01 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4479 % Solids: 92.42
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.116 - 0.0315
<br />1,2,3,7,8-PeCDD 0.596 - J 0.596 0.0468
<br />1,2,3,4,7,8-HxCDD 0.431 - J 0.0431 0.0503
<br />1,2,3,6,7,8-HxCDD 1.62 - J 0.162 0.0490 Total TCDD 2.23 -
<br />1,2,3,7,8,9-HxCDD 1.08 - J 0.108 0.0488 Total PeCDD 3.86 -J,M
<br />1,2,3,4,6,7,8-HpCDD 32.3 -0.323 0.0541 Total HxCDD 14.8 -
<br />OCDD 257 -0.0771 0.0888 Total HpCDD 63.0 -
<br />2,3,7,8-TCDF 1.95 -0.195 0.0243
<br />1,2,3,7,8-PeCDF 0.532 - J 0.0160 0.0285
<br />2,3,4,7,8-PeCDF 1.29 - J 0.387 0.0298
<br />1,2,3,4,7,8-HxCDF 2.13 - J 0.213 0.0255
<br />1,2,3,6,7,8-HxCDF 2.19 - J 0.219 0.0253
<br />2,3,4,6,7,8-HxCDF 1.23 - J 0.123 0.0279
<br />1,2,3,7,8,9-HxCDF 0.780 - J 0.0780 0.0367 Total TCDF 12.7 -
<br />1,2,3,4,6,7,8-HpCDF 13.5 -0.135 0.0321 Total PeCDF 10.5 -
<br />1,2,3,4,7,8,9-HpCDF 2.59 - J 0.0259 0.0396 Total HxCDF 14.2 -
<br />OCDF 20.3 -0.00609 0.0843 Total HpCDF 25.4 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 100 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 85.4 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 93.0 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 81.8 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 68.3 23.0 - 140
<br />13C-OCDD 56.9 17.0 - 157
<br />13C-2,3,7,8-TCDF 106 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 81.9 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 80.3 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 84.6 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 86.4 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 86.1 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 83.6 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 71.2 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 78.7 26.0 - 138
<br />13C-OCDF 57.1 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 97.5 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/25/2018
<br />5172 Hillsdale Circle * El Dorado Hills, CA 95762 * Tel (916) 934-0900 * Fax (916) 934-0999 * www.frontieranalytical.com
<br />4/26/2018
<br />of 000020000010
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