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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11455-005-SA Date Extracted: 04-27-2018 ICal: PCDDFAL4-12-20-17 Acquired: 04-30-2018
<br />Client ID: SP3-5 Date Received: 04-12-2018 GC Column: DB5MS 2005 WHO TEQ: 2.76
<br />Matrix: Solid Amount: 5.04 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4492 % Solids: 90.61
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.204 - 0.0273
<br />1,2,3,7,8-PeCDD 0.870 - J 0.870 0.0570
<br />1,2,3,4,7,8-HxCDD 0.714 - J 0.0714 0.0793
<br />1,2,3,6,7,8-HxCDD 2.01 - J 0.201 0.0940 Total TCDD 2.30 -
<br />1,2,3,7,8,9-HxCDD 1.56 - J 0.156 0.0823 Total PeCDD 7.61 -
<br />1,2,3,4,6,7,8-HpCDD 29.9 -0.299 0.0842 Total HxCDD 22.3 -
<br />OCDD 195 -0.0585 0.172 Total HpCDD 65.0 -
<br />2,3,7,8-TCDF 2.41 - F 0.241 0.0269
<br />1,2,3,7,8-PeCDF 0.523 - J 0.0157 0.0449
<br />2,3,4,7,8-PeCDF 1.00 - J 0.300 0.0468
<br />1,2,3,4,7,8-HxCDF 1.17 - J 0.117 0.0437
<br />1,2,3,6,7,8-HxCDF 1.47 - J 0.147 0.0417
<br />2,3,4,6,7,8-HxCDF 0.968 - J 0.0968 0.0574
<br />1,2,3,7,8,9-HxCDF 0.495 - J 0.0495 0.0657 Total TCDF 11.3 -
<br />1,2,3,4,6,7,8-HpCDF 11.1 -0.111 0.0747 Total PeCDF 8.69 -
<br />1,2,3,4,7,8,9-HpCDF 1.63 - J 0.0163 0.0883 Total HxCDF 12.1 -
<br />OCDF 16.6 -0.00498 0.170 Total HpCDF 20.9 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 90.8 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 98.5 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 96.9 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 96.6 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 90.3 23.0 - 140
<br />13C-OCDD 80.2 17.0 - 157
<br />13C-2,3,7,8-TCDF 95.9 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 94.0 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 94.5 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 89.5 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 88.0 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 86.7 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 87.4 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 87.4 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 87.6 26.0 - 138
<br />13C-OCDF 78.4 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 88.5 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />5/1/2018 5/1/2018
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