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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11455-013-SA Date Extracted: 04-27-2018 ICal: PCDDFAL4-12-20-17 Acquired: 05-01-2018
<br />Client ID: SP4-1 Date Received: 04-12-2018 GC Column: DB5MS 2005 WHO TEQ: 2.91
<br />Matrix: Solid Amount: 5.04 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4492 % Solids: 96.08
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.184 - 0.0273
<br />1,2,3,7,8-PeCDD ND 0.309 -0.0570
<br />1,2,3,4,7,8-HxCDD 0.471 - J 0.0471 0.0793
<br />1,2,3,6,7,8-HxCDD 4.20 - J 0.420 0.0940 Total TCDD 0.754 -J
<br />1,2,3,7,8,9-HxCDD 1.88 - J 0.188 0.0823 Total PeCDD 1.40 -J
<br />1,2,3,4,6,7,8-HpCDD 79.8 -0.798 0.0842 Total HxCDD 32.4 -
<br />OCDD 683 -0.205 0.172 Total HpCDD 150 -
<br />2,3,7,8-TCDF 1.73 -0.173 0.0269
<br />1,2,3,7,8-PeCDF 0.461 - J 0.0138 0.0449
<br />2,3,4,7,8-PeCDF 1.02 - J 0.306 0.0468
<br />1,2,3,4,7,8-HxCDF 1.81 - J 0.181 0.0437
<br />1,2,3,6,7,8-HxCDF 1.98 - J 0.198 0.0417
<br />2,3,4,6,7,8-HxCDF 1.53 - J 0.153 0.0574
<br />1,2,3,7,8,9-HxCDF 0.615 - J 0.0615 0.0657 Total TCDF 12.4 -
<br />1,2,3,4,6,7,8-HpCDF 13.8 -0.138 0.0747 Total PeCDF 7.70 -
<br />1,2,3,4,7,8,9-HpCDF 2.31 - J 0.0231 0.0883 Total HxCDF 16.5 -
<br />OCDF 24.5 -0.00735 0.170 Total HpCDF 31.6 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 88.8 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 92.7 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 92.9 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 89.9 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 86.4 23.0 - 140
<br />13C-OCDD 78.9 17.0 - 157
<br />13C-2,3,7,8-TCDF 94.0 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 89.8 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 92.5 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 81.9 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 81.2 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 80.1 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 82.0 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 82.5 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 86.5 26.0 - 138
<br />13C-OCDF 78.1 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 85.3 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />5/1/2018 5/1/2018
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