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Brusca File No. 137-002 <br />Page 6 <br />December 14, 2018 <br />Murphy Parkway Property Waste Materials Management Verification Report <br /> <br /> <br />• Total Petroleum Hydrocarbons as gasoline, diesel, and motor oil by EPA Method 8015B <br />• SVOCs by EPA Method 8270C <br />• Polychlorinated Biphenyls (PCBs) by EPA Method 8082 <br />• Title 22 Metals Total Threshold Limit (TTLC) by EPA Method 6010/200.7 <br />• Arsenic and Lead by EPA Method 6010 <br />• Dioxins and Furans by EPA Method E1613 <br /> <br />The results of the above-listed analyses performed on verification soil samples collected beneath <br />WU1 are summarized on Tables I through III; the laboratory reports and chain-of-custody <br />documentation are included in the appendix of this report. For reference, hazardous waste criteria <br />and screening levels established in the approved EMMP are included on the summary data tables. <br /> <br />As shown on Tables I through III and the appended laboratory reports, none of the verification soil <br />samples collected beneath the removed WU1 materials contained any of the tested analytes at <br />concentrations above hazardous waste criteria or above the established/approved screening values <br />for commercial/industrial site usage. As such, the verification soil sampling/testing results indicate <br />that the WU1 removal activities were successful, and residual soil conditions in this area do not <br />pose an unacceptable risk, considering future commercial/industrial site usage. <br /> <br />4.4 Removed Wastes/Stockpiles Sampling and Testing <br /> <br />Per the provisions of the EMMP and Addendum, our firm also collected samples of the <br />removed/stockpiled wastes from the WU1 area for analytical laboratory testing. The sampling was <br />conducted by a Certified Engineering Geologist from our firm and was overseen by regulatory <br />agency representatives. A total of 49 spatially distributed, random/representative samples of the <br />WU1 materials was collected. The samples were placed in laboratory-provided glass jars, <br />immediately placed on ice, and transported to State-certified analytical laboratories under chain- <br />of-custody for analysis. Each sample was analyzed for the following: <br /> <br />• Total Petroleum Hydrocarbons as gasoline, diesel, and motor oil by EPA Method 8015B <br />• SVOCs by EPA Method 8270C <br />• Polychlorinated Biphenyls (PCBs) by EPA Method 8082 <br />• Title 22 Metals Total Threshold Limit (TTLC) by EPA Method 6010/200.7 <br />• Dioxins and Furans by EPA Method E1613 <br /> <br />As outlined in the EMMP, samples of stockpiled materials from WU1 containing the highest <br />concentrations of total metals were analyzed for soluble Title 22 metals by the Waste Extraction <br />Method (WET) by EPA Method 1311 using deionized water (DI) as the extractant; this element <br />of the testing program was required by the CVRWQCB for the purpose of evaluating potential <br />future leaching impact to groundwater posed by the waste materials. A total of 11 samples was <br />selected for the DI WET metals testing, including samples from each of the five stockpiles. <br /> <br />The results of the above-listed analyses performed on samples of removed/stockpiled wastes from <br />WU1 are summarized on Tables IV through VII; the laboratory reports and chain-of-custody <br />documentation are included in the appendix of this report. For reference, hazardous waste criteria <br />and screening levels established in the approved EMMP are included on the summary data tables.