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Client Sample Results Client: Union Pacific RR Operations eProcurement Job ID: 440-248216-1 Project/Site: UPRR-Sludge Bin Stockton- New Profile Client Sample ID: Sludge Bin-Stockton Lab Sample ID: 440-248216-1 Date Collected: 08/15/19 05:30 Matrix: Waste Date Received: 08/16/19 14:09 Method: 8260B -Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac trans-1,2-Dichloroethene ND 880 440 ug/Kg 08/22/1915:01 08/27/1913:09 100 trans-1,3-Dichloropropene ND 880 440 ug/Kg 08/22/1915:01 08/27/1913:09 100 Trichloroethene ND 880 440 ug/Kg 08/22/1915:01 08/27/1913:09 100 Trichlorofluoromethane ND 2200 880 ug/Kg 08/22/1915:01 08/27/1913:09 100 Vinyl chloride ND 2200 880 ug/Kg 08/22/19 15:01 08/27/19 13:09 100 1,2-Dibromoethane(EDB) ND 880 440 ug/Kg 08/22/19 15:01 08/27/19 13:09 100 Bromochloromethane ND 2200 880 ug/Kg 08/22/1915:01 08/27/1913:09 100 Bromodichloromethane ND 880 440 ug/Kg 08/22/1915:01 08/27/1913:09 100 Dibromochloromethane ND 880 440 ug/Kg 08/22/1915:01 08/27/1913:09 100 p-Isopropyltoluene ND 880 440 ug/Kg 08/22/1915:01 08/27/1913:09 100 2-Butanone(MEK) ND 8800 4400 ug/Kg 08/22/19 15:01 08/27/19 13:09 100 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Toluene-d8(Surr) 94 60-140 08/22/19 15:01 08/27/19 13:09 100 4-Bromofluorobenzene(Surr) 87 65-140 08/22/19 15:01 08/27/19 13:09 100 Dibromofluoromethane(Surr) 102 55-140 08/22/19 15:01 08/27/19 13:09 100 Method: 8270C -Semivolatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,2,4-Trichlorobenzene ND 22 8.8 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 1,3-Dichlorobenzene ND 22 8.8 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 1,4-Dichlorobenzene ND 22 8.8 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 2,4,5-Trichlorophenol ND 44 8.8 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 2,4,6-Trichlorophenol ND 44 5.3 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 2,4-Dichlorophenol ND 22 5.3 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 2,4-Dimethylphenol ND 22 8.8 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 2,4-Dinitrophenol ND 88 22 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 2,4-Dinitrotoluene ND 22 5.3 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 2,6-Dinitrotoluene ND 22 7.1 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 2-Chloronaphthalene ND 22 5.3 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 2-Chlorophenol ND 22 5.3 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 2-Methylnaphthalene ND 22 5.3 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 2-Methylphenol ND 22 5.3 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 2-Nitroaniline ND 22 5.3 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 2-Nitrophenol ND 22 8.8 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 3,3'-Dichlorobenzidine ND 56 11 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 3-Nitroaniline ND 22 8.8 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 4,6-Dinitro-2-methylphenol ND 28 8.8 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 4-Bromophenyl phenyl ether ND 22 5.3 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 4-Chloro-3-methylphenol ND 22 5.3 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 4-Chloroaniline ND 22 8.8 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 4-Chlorophenyl phenyl ether ND 22 6.2 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 3-Methylphenol+4-Methylphenol ND 22 8.8 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 4-Nitroaniline ND 56 8.8 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 4-Nitrophenol ND 56 9.7 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 Acenaphthene ND 22 5.3 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 Acenaphthylene ND 22 5.3 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 Aniline ND 28 6.2 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 Anthracene ND 22 5.3 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 Benzidine ND 89 44 mg/Kg 08/20/19 12:20 08/21/19 01:51 1 Eurofins TestAmerica, Irvine Page 6 of 32 8/30/2019