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QC Sample Results <br /> Client: Union Pacific RR Operations eProcurement Job ID: 440-248216-1 <br /> Project/Site: UPRR-Sludge Bin Stockton- New Profile <br /> Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued) <br /> Lab Sample ID: MB 440-564322/1-A Client Sample ID: Method Blank <br /> Matrix: Waste Prep Type: Total/NA <br /> Analysis Batch: 564438 Prep Batch: 564322 <br /> MB MB <br /> Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac <br /> Phenol-d6(Surr) 90 70-130 08/20/19 12:20 08/20/19 21:40 1 <br /> Lab Sample ID: LCS 440-564322/2-A Client Sample ID: Lab Control Sample <br /> Matrix: Waste Prep Type: Total/NA <br /> Analysis Batch: 564438 Prep Batch: 564322 <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> 1,2,4-Trichlorobenzene 250 255 mg/Kg 102 73-121 <br /> 1,3-Dichlorobenzene 250 262 mg/Kg 105 74-121 <br /> 1,4-Dichlorobenzene 250 269 mg/Kg 108 70-130 <br /> 2,4,5-Trichlorophenol 250 267 mg/Kg 107 67-126 <br /> 2,4,6-Trichlorophenol 250 264 mg/Kg 106 75-121 <br /> 2,4-Dichlorophenol 250 270 mg/Kg 108 71-125 <br /> 2,4-Dimethylphenol 250 272 mg/Kg 109 73-120 <br /> 2,4-Dinitrophenol 500 558 mg/Kg 112 58-140 <br /> 2,4-Dinitrotoluene 250 268 mg/Kg 107 60-140 <br /> 2,6-Dinitrotoluene 250 268 mg/Kg 107 79-121 <br /> 2-Chloronaphthalene 250 274 mg/Kg 109 70-126 <br /> 2-Chlorophenol 250 272 mg/Kg 109 69-126 <br /> 2-Methylnaphthalene 250 263 mg/Kg 105 75-120 <br /> 2-Methylphenol 250 276 mg/Kg 111 61-133 <br /> 2-Nitroaniline 250 271 mg/Kg 108 62-135 <br /> 2-Nitrophenol 250 298 mg/Kg 119 76-126 <br /> 3,3'-Dichlorobenzidine 250 241 mg/Kg 96 30-170 <br /> 3-Nitroaniline 250 190 mg/Kg 76 60-140 <br /> 4,6-Dinitro-2-methylphenol 500 588 mg/Kg 118 62-138 <br /> 4-Bromophenyl phenyl ether 250 265 mg/Kg 106 75-125 <br /> 4-Chloro-3-methylphenol 250 252 mg/Kg 101 69-121 <br /> 4-Chloroaniline 250 123 mg/Kg 49 71-128 <br /> 4-Chlorophenyl phenyl ether 250 239 mg/Kg 96 77-120 <br /> 3-Methylphenol+4-Methylphenol 250 259 mg/Kg 104 66-132 <br /> 4-Nitroaniline 250 255 mg/Kg 102 40-160 <br /> 4-Nitrophenol 500 439 mg/Kg 88 50-145 <br /> Acenaphthene 250 268 mg/Kg 107 69-122 <br /> Acenaphthylene 250 270 mg/Kg 108 78-116 <br /> Aniline 250 213 mg/Kg 85 57-132 <br /> Anthracene 250 273 mg/Kg 109 74-122 <br /> Benzidine 250 153 mg/Kg 61 20-180 <br /> Benzo[a]anthracene 250 293 mg/Kg 117 73-123 <br /> Benzo[a]pyrene 250 279 mg/Kg 112 78-108 <br /> Benzo[b]fluoranthene 250 277 mg/Kg 111 69-120 <br /> Benzo[g,h,i]perylene 250 319 mg/Kg 128 40-160 <br /> Benzo[k]fluoranthene 250 254 mg/Kg 102 80-120 <br /> Benzoic acid 250 275 mg/Kg 110 55-140 <br /> Benzyl alcohol 250 253 mg/Kg 101 35-139 <br /> Bis(2-chloroethoxy)methane 250 251 mg/Kg 100 66-124 <br /> Bis(2-chloroethyl)ether 250 241 mg/Kg 96 56-133 <br /> Bis(2-ethylhexyl)phthalate 250 328 mg/Kg 131 60-132 <br /> Eurofins TestAmerica, Irvine <br /> Page 17 of 32 8/30/2019 <br />