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QC Sample Results Client: Union Pacific RR Operations eProcurement Job ID: 440-248216-1 Project/Site: UPRR-Sludge Bin Stockton- New Profile Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCSD 440-564322/3-A Client Sample ID: Lab Control Sample Dup Matrix: Waste Prep Type: Total/NA Analysis Batch: 564438 Prep Batch: 564322 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit 2,4-Dinitrophenol 500 526 mg/Kg 105 —68-14-0 6 35 2,4-Dinitrotoluene 250 264 mg/Kg 106 60-140 1 35 2,6-Dinitrotoluene 250 259 mg/Kg 103 79-121 4 35 2-Chloronaphthalene 250 260 mg/Kg 104 70-126 5 35 2-Chlorophenol 250 262 mg/Kg 105 69-126 4 35 2-Methylnaphthalene 250 251 mg/Kg 100 75-120 5 35 ' 2-Methylphenol 250 259 mg/Kg 104 61-133 6 35 2-Nitroaniline 250 255 mg/Kg 102 62-135 6 35 2-Nitrophenol 250 287 mg/Kg 115 76-126 4 35 3,3'-Dichlorobenzidine 250 230 mg/Kg 92 30-170 4 35 3-Nitroaniline 250 189 mg/Kg 76 60-140 1 35 4,6-Dinitro-2-methylphenol 500 545 mg/Kg 109 62-138 8 35 4-Bromophenyl phenyl ether 250 247 mg/Kg 99 75-125 7 35 4-Chloro-3-methylphenol 250 242 mg/Kg 97 69-121 4 35 4-Chloroaniline 250 122 mg/Kg 49 71-128 1 35 4-Chlorophenyl phenyl ether 250 230 mg/Kg 92 77-120 4 35 3-Methylphenol+4-Methylphenol 250 250 mg/Kg 100 66-132 3 35 4-Nitroaniline 250 239 mg/Kg 96 40-160 7 35 4-Nitrophenol 500 422 mg/Kg 84 50-145 4 35 Acenaphthene 250 256 mg/Kg 102 69-122 5 35 Acenaphthylene 250 260 mg/Kg 104 78-116 4 35 Aniline 250 206 mg/Kg 83 57-132 3 35 Anthracene 250 260 mg/Kg 104 74-122 5 35 Benzidine 250 141 mg/Kg 56 20-180 8 35 Benzo[a]anthracene 250 280 mg/Kg 112 73-123 4 35 Benzo[a]pyrene 250 266 mg/Kg 106 78-108 5 35 Benzo[b]fluoranthene 250 255 mg/Kg 102 69-120 8 35 Benzo[g,h,i]perylene 250 312 mg/Kg 125 40-160 2 35 Benzo[k]fluoranthene 250 251 mg/Kg 100 80-120 1 35 Benzoic acid 250 277 mg/Kg 111 55-140 1 35 Benzyl alcohol 250 241 mg/Kg 96 35-139 5 35 Bis(2-chloroethoxy)methane 250 238 mg/Kg 95 66-124 5 35 Bis(2-chloroethyl)ether 250 229 mg/Kg 92 56-133 5 35 Bis(2-ethylhexyl)phthalate 250 308 mg/Kg 123 60-132 6 35 Butyl benzyl phthalate 250 290 mg/Kg 116 62-135 8 35 Chrysene 250 274 mg/Kg 109 73-123 4 35 Dibenz(a,h)anthracene 250 265 mg/Kg 106 40-160 4 35 Dibenzofuran 250 253 mg/Kg 101 77-120 3 35 Diethyl phthalate 250 241 mg/Kg 96 65-135 4 35 Dimethyl phthalate 250 245 mg/Kg 98 77-120 5 35 Di-n-butyl phthalate 250 265 mg/Kg 106 74-123 5 35 Di-n-octyl phthalate 250 304 mg/Kg 122 62-138 7 35 Fluoranthene 250 252 mg/Kg 101 74-123 5 35 Fluorene 250 246 mg/Kg 98 75-124 3 35 Hexachlorobenzene 250 249 mg/Kg 100 70-130 7 35 Hexachlorobutadiene 250 218 mg/Kg 87 68-131 6 35 Hexachlorocyclopentadiene 250 224 mg/Kg 90 19-130 7 35 Hexachloroethane 250 239 mg/Kg 96 69-130 6 35 Indeno[1,2,3-cd]pyrene 250 276 mg/Kg 110 50-150 2 35 Eurofins TestAmerica, Irvine Page 19 of 32 8/30/2019