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QC Sample Results <br /> Client: Union Pacific RR Operations eProcurement Job ID: 440-248216-1 <br /> Project/Site: UPRR-Sludge Bin Stockton- New Profile <br /> Method: 8015B - Gasoline Range Organics - (GC) (Continued) <br /> Lab Sample ID: LCSD 440-563995/4 Client Sample ID: Lab Control Sample Dup <br /> Matrix: Waste Prep Type: Total/NA <br /> Analysis Batch: 563995 <br /> Spike LCSD LCSD %Rec. RPD <br /> Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> GRO(C4-C12) 160000 127000 ug/Kg 80 70-135 2 20 <br /> LCSD LCSD <br /> Surrogate %Recovery Qualifier Limits <br /> 4-Bromofluorobenzene(Burr) 100 65-140 <br /> Method: 6010B - Metals (ICP) <br /> Lab Sample ID: MB 440-565089/1-A ^5 Client Sample ID: Method Blank <br /> Matrix: Waste Prep Type: Total/NA <br /> Analysis Batch: 565295 Prep Batch: 565089 <br /> MB MB <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> Antimony ND 9.9 5.0 mg/Kg 08/23/1910:01 08/24/1916:24 5 <br /> Arsenic ND 3.0 1.5 mg/Kg 08/23/1910:01 08/24/1916:24 5 <br /> Barium ND 1.5 0.74 mg/Kg 08/23/1910:01 08/24/1916:24 5 <br /> Beryllium ND 0.50 0.25 mg/Kg 08/23/1910:01 08/24/1916:24 5 <br /> Cadmium ND 0.50 0.25 mg/Kg 08/23/1910:01 08/24/1916:24 5 <br /> Chromium ND 0.99 0.50 mg/Kg 08/23/1910:01 08/24/1916:24 5 <br /> Cobalt ND 0.99 0.50 mg/Kg 08/23/1910:01 08/24/1916:24 5 <br /> Copper ND 2.0 1.1 mg/Kg 08/23/1910:01 08/24/1916:24 5 <br /> Lead ND 2.0 0.99 mg/Kg 08/23/1910:01 08/24/1916:24 5 <br /> Molybdenum ND 2.0 0.99 mg/Kg 08/23/1910:01 08/24/1916:24 5 <br /> Nickel ND 2.0 0.99 mg/Kg 08/23/1910:01 08/24/1916:24 5 <br /> Selenium ND 3.0 1.7 mg/Kg 08/23/1910:01 08/24/1916:24 5 <br /> Thallium ND 9.9 5.0 mg/Kg 08/23/1910:01 08/24/1916:24 5 <br /> Vanadium ND 0.99 0.50 mg/Kg 08/23/1910:01 08/24/1916:24 5 <br /> Zinc ND 5.0 2.5 mg/Kg 08/23/1910:01 08/24/1916:24 5 <br /> Lab Sample ID: LCS 440-565089/2-A ^5 Client Sample ID: Lab Control Sample <br /> Matrix: Waste Prep Type: Total/NA <br /> Analysis Batch: 565295 Prep Batch: 565089 <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> Antimony 49.5 48.0 mg/Kg 97 80-120 <br /> Arsenic 49.5 45.1 mg/Kg 91 80-120 <br /> Barium 49.5 47.2 mg/Kg 95 80-120 <br /> Beryllium 49.5 44.6 mg/Kg 90 80-120 <br /> Cadmium 49.5 45.2 mg/Kg 91 80-120 <br /> Chromium 49.5 46.6 mg/Kg 94 80-120 <br /> Cobalt 49.5 46.2 mg/Kg 93 80-120 <br /> Copper 49.5 46.0 mg/Kg 93 80-120 <br /> Lead 49.5 46.2 mg/Kg 93 80-120 <br /> Molybdenum 49.5 47.4 mg/Kg 96 80-120 <br /> Nickel 49.5 46.1 mg/Kg 93 80-120 <br /> Selenium 49.5 42.0 mg/Kg 85 80-120 <br /> Thallium 49.5 43.0 mg/Kg 87 80-120 <br /> Vanadium 49.5 45.8 mg/Kg 93 80-120 <br /> Zinc 49.5 45.5 mg/Kg 92 80-120 <br /> Eurofins TestAmerica, Irvine <br /> Page 21 of 32 8/30/2019 <br />