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SAMPLE #2 SAND SAMPLE RESULTS - 02 ONE LAB.NATIONWIDE. Collected date/time: 04/29/20 11:30 L1213730 Volatile Organic Compounds (GC/MS) by Method 82608 Result Qualifier MDL RDL Dilution Analysis Batch FpAnalyte mg/kg mg/kg mg/kg date/time 1,2-Dibromo-3-Chloropropane U 0.00390 0.0250 1 05/03/202017:43 WG1469977 FTc 1,2-Dibromoethane U 0.000648 0.00250 1 05/03/202017:43 WG1469977 Dibromomethane U 0.000750 0.00500 1 05/03/202017:43 WG1469977 FS 1,2-Dichlorobenzene U 0.000425 0.00500 1 05/03/202017:43 WG1469977 1,3-Dichlorobenzene U 0.000600 0.00500 1 05/03/202017:43 WG1469977 1,4-Dichlorobenzene U 0.000700 0.00500 1 05/03/202017:43 WG1469977 [Cn] Dichlorodifluoromethane U 0.00161 0.00250 1 05/03/202017:43 WG1469977 1,1-Dichloroethane U 0.000491 0.00250 1 05/03/202017:43 WG1469977 1,2-Dichloroethane U 0.000649 0.00250 1 05/03/202017:43 WG1469977 1,1-Dichloroethene U 0.000606 0.00250 1 05/03/202017:43 WG1469977 cis-1,2-Dichloroethene U 0.000734 0.00250 1 05/03/202017:43 WG1469977 Fc trans-1,2-Dichloroethene U 0.00104 0.00500 1 05/03/2020 17:43 WG1469977 1,2-Dichloropropane U 0.00142 0.00500 1 05/03/202017:43 WG1469977 7 1,1-Dichloropropene U 0.000809 0.00250 1 05/03/202017:43 WG1469977 ql 1,3-Dichloropropane U 0.000501 0.00500 1 05/03/202017:43 WG1469977 cis-1,3-Dichloropropene U 0.000757 0.00250 1 05/03/202017:43 WG1469977 FAI trans-1,3-Dichloropropene U 0.00114 0.00500 1 05/03/202017:43 WG1469977 2,2-Dichloropropane U 0.00138 0.00250 1 05/03/202017:43 WG1469977 FSC Di-isopropyl ether U 0.000410 0.00100 1 05/03/202017:43 WG1469977 Ethylbenzene 0.00680 0.000737 0.00250 1 05/03/202017:43 WG1469977 Hexachloro-1,3-butadiene U 0.00600 0.0250 1 05/03/202017:43 WG1469977 Isopropylbenzene 0.00366 0.000425 0.00250 1 05/03/202017:43 WG1469977 p-Isopropyltoluene 0.00671 0.00255 0.00500 1 05/03/202017:43 WG1469977 2-Butanone(MEK) 0.186 0.0635 0.100 1 05/03/202017:43 WG1469977 Methylene Chloride U 0.00664 0.0250 1 05/03/202017:43 WG1469977 4-Methyl-2-pentanone(MIBK) 0.224 0.00228 0.0250 1 05/03/202017:43 WG1469977 Methyl tert-butyl ether U 0.000350 0.00100 1 05/03/202017:43 WG1469977 Naphthalene 0.391 0.00488 0.0125 1 05/03/202017:43 WG1469977 n-Propylbenzene 0.0313 0.000950 0.00500 1 05/03/202017:43 WG1469977 Styrene 0.00182 J 0.000229 0.0125 1 05/03/202017:43 WG1469977 1,1,1,2-Tetrachloroethane U 0.000948 0.00250 1 05/03/202017:43 WG1469977 1,1,2,2-Tetrachloroethane U 0.000695 0.00250 1 05/03/202017:43 WG1469977 1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250 1 05/03/202017:43 WG1469977 Tetrachloroethene U 0.000896 0.00250 1 05/03/202017:43 WG1469977 Toluene 0.00724 0.00130 0.00500 1 05/03/202017:43 WG1469977 1,2,3-Trichlorobenzene U 0.00733 0.0125 1 05/03/2020 17:43 WG1469977 1,2,4-Trichlorobenzene U 0.00440 0.0125 1 05/03/2020 17:43 WG1469977 1,1,1-Trichloroethane U 0.000923 0.00250 1 05/03/202017:43 WG1469977 1,1,2-Trichloroethane U 0.000597 0.00250 1 05/03/202017:43 WG1469977 Trichloroethene U 0.000584 0.00100 1 05/03/202017:43 WG1469977 Trichlorofluoromethane U 0.000827 0.00250 1 05/03/202017:43 WG1469977 1,2,3-Trichloropropane U 0.00162 0.0125 1 05/03/202017:43 WG1469977 1,2,4-Trimethylbenzene 0.630 0.00158 0.00500 1 05/03/202017:43 WG1469977 1,2,3-Trim ethyl benzene 0.249 0.00158 0.00500 1 05/03/202017:43 WG1469977 1,3,5-Trim ethyl benzene 0.133 0.00200 0.00500 1 05/03/202017:43 WG1469977 Vinyl chloride U 0.00116 0.00250 1 05/03/202017:43 WG1469977 Xylenes,Total 0.0785 0.000880 0.00650 1 05/03/202017:43 WG1469977 (S)Toluene-d8 111 75.0-131 05/03/202017.43 WG1469977 (S)4-Bromofluorobenzene 105 67.0-138 05/03/202017.43 WG1469977 (S)1,2-Dich/oroethone-d4 75.1 70.0-130 05/03/2020171-43 WG1469977 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-Patriot Environmental Services MODESTO,CERES CA L1213730 05/05/20 19:35 10 of 56