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SAMPLE #4 MOTOR OIL SAMPLE RESULTS - 04 ONE LAB.NATIONWIDE. Collected date/time: 04/29/20 11:50 L1213730 Volatile Organic Compounds (GC/MS) by Method 82608 Result Qualifier MDL RDL Dilution Analysis Batch FpAnalyte mg/kg mg/kg mg/kg date/time Bromodichloromethane U 0.0580 0.200 80 05/04/202017:49 WG1470010 FTc Bromoform U 0.0936 2.00 80 05/04/202017:49 WG1470010 Bromomethane U 0.158 1.00 80 05/04/202017:49 WG1470010 FS n-Butylbenzene 2.95 0.420 1.00 80 05/04/202017:49 WG1470010 sec-Butyl benzene 0.705 J 0.230 1.00 80 05/04/202017:49 WG1470010 tert-Butylbenzene U 0.156 0.400 80 05/04/202017:49 WG1470010 Fn Carbon tetrachloride U 0.0718 0.400 80 05/04/202017:49 WG1470010 Chlorobenzene U 0.0168 0.200 80 05/04/202017:49 WG1470010 Chlorodibromomethane U 0.0490 0.200 80 05/04/202017:49 WG1470010 Chloroethane U 0.136 0.400 80 05/04/202017:49 WG1470010 Chloroform U 0.0824 0.200 80 05/04/202017:49 WG1470010 Fc Chloromethane U 0.348 1.00 80 05/04/202017:49 WG1470010 2-Chlorotoluene U 0.0692 0.200 80 05/04/202017:49 WG1470010 4-Chlorotoluene U 0.0360 0.400 80 05/04/202017:49 WG1470010 ql 1,2-Dibromo-3-Chloropropane U 0.312 2.00 80 05/04/202017:49 WG1470010 1,2-Dibromoethane U 0.0518 0.200 80 05/04/202017:49 WG1470010 FAI Dibromomethane U 0.0600 0.400 80 05/04/202017:49 WG1470010 1,2-Dichlorobenzene U 0.0340 0.400 80 05/04/202017:49 WG1470010 FSC 1,3-Dichlorobenzene U 0.0480 0.400 80 05/04/202017:49 WG1470010 1,4-Dichlorobenzene U 0.0560 0.400 80 05/04/202017:49 WG1470010 Dichlorodifluoromethane U 0.129 0.200 80 05/04/202017:49 WG1470010 1,1-Dichloroethane U 0.0393 0.200 80 05/04/202017:49 WG1470010 1,2-Dichloroethane U 0.0519 0.200 80 05/04/202017:49 WG1470010 1,1-Dichloroethene U 0.0485 0.200 80 05/04/202017:49 WG1470010 cis-1,2-Dichloroethene U 0.0587 0.200 80 05/04/202017:49 WG1470010 trans-1,2-Dichloroethene U 0.0832 0.400 80 05/04/202017:49 WG1470010 1,2-Dichloropropane U 0.114 0.400 80 05/04/202017:49 WG1470010 1,1-Dichloropropene U 0.0647 0.200 80 05/04/202017:49 WG1470010 1,3-Dichloropropane U 0.0401 0.400 80 05/04/202017:49 WG1470010 cis-1,3-Dichloropropene U 0.0606 0.200 80 05/04/202017:49 WG1470010 trans-1,3-Dichloropropene U 0.0912 0.400 80 05/04/202017:49 WG1470010 2,2-Dichloropropane U 0.110 0.200 80 05/04/202017:49 WG1470010 Di-isopropyl ether U 0.0328 0.0800 80 05/04/202017:49 WG1470010 Ethylbenzene 7.99 0.0590 0.200 80 05/04/202017:49 WG1470010 Hexachloro-1,3-butadiene U 0.480 2.00 80 05/04/202017:49 WG1470010 Isopropylbenzene 0.983 0.0340 0.200 80 05/04/202017:49 WG1470010 p-Isopropyltoluene 0.448 0.204 0.400 80 05/04/202017:49 WG1470010 2-Butanone(MEK) U 5.08 8.00 80 05/04/202017:49 WG1470010 Methylene Chloride U 0.531 2.00 80 05/04/202017:49 WG1470010 4-Methyl-2-pentanone(MIBK) U 0.182 2.00 80 05/04/202017:49 WG1470010 Methyl tert-butyl ether U 0.0280 0.0800 80 05/04/202017:49 WG1470010 Naphthalene 27.8 0.390 1.00 80 05/04/202017:49 WG1470010 n-Propylbenzene 4.82 0.0760 0.400 80 05/04/202017:49 WG1470010 Styrene U 0.0183 1.00 80 05/04/202017:49 WG1470010 1,1,1,2-Tetrachloroethane U 0.0758 0.200 80 05/04/202017:49 WG1470010 1,1,2,2-Tetrachloroethane U 0.0556 0.200 80 05/04/202017:49 WG1470010 1,1,2-Trichlorotrifluoroethane U 0.0603 0.200 80 05/04/202017:49 WG1470010 Tetrachloroethene U 0.0717 0.200 80 05/04/202017:49 WG1470010 Toluene 15.0 0.104 0.400 80 05/04/202017:49 WG1470010 1,2,3-Trichlorobenzene U 0.586 1.00 80 05/04/202017:49 WG1470010 1,2,4-Trichlorobenzene U 0.352 1.00 80 05/04/202017:49 WG1470010 1,1,1-Trichloroethane U 0.0738 0.200 80 05/04/202017:49 WG1470010 1,1,2-Trichloroethane U 0.0478 0.200 80 05/04/202017:49 WG1470010 Trichloroethene U 0.0467 0.0800 80 05/04/202017:49 WG1470010 Trichlorofluoromethane U 0.0662 0.200 80 05/04/202017:49 WG1470010 1,2,3-Trichloropropane U 0.130 1.00 80 05/04/202017:49 WG1470010 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-Patriot Environmental Services MODESTO,CERES CA L1213730 05/05/20 19:35 18 of 56