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WG1469759 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 82606 L1213730-03 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) FP1(LCS)R3524160-1 05/02/2019:31•(LCSD)R3524160-3 05/02/20 21:12 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits FTC Analyte mg/kg mg/kg mg/kg % % % % % Naphthalene 0.125 0.0966 0.0930 77.3 74.4 59.0-130 3.80 20 n-Propylbenzene 0.125 0.143 0.137 114 110 74.0-126 4.29 20 3 SS Styrene 0.125 0.178 0.184 142 147 72.0-127 J4 J4 3.31 20 1,1,1,2-Tetrachloroethane 0.125 0.125 0.130 100 104 74.0-129 3.92 20 rCn 1,1,2,2-Tetrachloroethane 0.125 0.143 0.144 114 115 68.0-128 0.697 20 Tetrachloroethene 0.125 0.134 0.129 107 103 70.0-136 3.80 20 Toluene 0.125 0.122 0.124 97.6 99.2 75.0-121 1.63 20 FSr 1,1,2-Trichlorotrifluoroethane 0.125 0.129 0.128 103 102 61.0-139 0.778 20 1,2,3-Trichlorobenzene 0.125 0.105 0.0947 84.0 75.8 59.0-139 10.3 20 1,2,4-Trichlorobenzene 0.125 0.103 0.103 82.4 82.4 62.0-137 0.000 20 1,1,1-Trichloroethane 0.125 0.116 0.107 92.8 85.6 69.0-126 8.07 20 1,1,2-Trichloroethane 0.125 0.115 0.123 92.0 98.4 78.0-123 6.72 20 7G1 Trichloroethene 0.125 0.117 0.115 93.6 92.0 76.0-126 1.72 20 Trichlorofluoromethane 0.125 0.111 0.105 88.8 84.0 61.0-142 5.56 20 1,2,3-Trichloropropane 0.125 0.133 0.142 106 114 67.0-129 6.55 20 FAI 1,2,3-Trim ethyl benzene 0.125 0.147 0.141 118 113 74.0-124 4.17 20 1,2,4-Trimethylbenzene 0.125 0.122 0.114 97.6 91.2 70.0-126 6.78 20 FSC 1,3,5-Trim ethyl benzene 0.125 0.118 0.111 94.4 88.8 73.0-127 6.11 20 Vinyl chloride 0.125 0.160 0.159 128 127 63.0-134 0.627 20 Xylenes,Total 0.375 0.435 0.447 116 119 72.0-127 2.72 20 (S)Toluene-d8 110 109 75.0-131 (S)4-Bromofluorobenzene 104 109 670-138 (S)1,2-Dich/oroethone-d4 90.0 87.6 70.0-130 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-Patriot Environmental Services MODESTO,CERES CA L1213730 05/05/20 19:35 33 of 56