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WG1469977 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 82606 L1213730-01,02 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) FP1(LCS)R3524320-1 05/03/2011:12•(LCSD)R3524320-2 05/03/2011:32 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits FTC Analyte mg/kg mg/kg mg/kg % % % % % Naphthalene 0.125 0.124 0.123 99.2 98.4 59.0-130 0.810 20 n-Propylbenzene 0.125 0.122 0.126 97.6 101 74.0-126 3.23 20 FSS Styrene 0.125 0.131 0.132 105 106 72.0-127 0.760 20 1,1,1,2-Tetrachloroethane 0.125 0.125 0.126 100 101 74.0-129 0.797 20 rCn 1,1,2,2-Tetrachloroethane 0.125 0.115 0.119 92.0 95.2 68.0-128 3.42 20 Tetrachloroethene 0.125 0.140 0.140 112 112 70.0-136 0.000 20 Toluene 0.125 0.120 0.123 96.0 98.4 75.0-121 2.47 20 FSr 1,1,2-Trichlorotrifluoroethane 0.125 0.174 0.167 139 134 61.0-139 4.11 20 1,2,3-Trichlorobenzene 0.125 0.130 0.126 104 101 59.0-139 3.12 20 1,2,4-Trichlorobenzene 0.125 0.135 0.138 108 110 62.0-137 2.20 20 1,1,1-Trichloroethane 0.125 0.135 0.137 108 110 69.0-126 1.47 20 1,1,2-Trichloroethane 0.125 0.119 0.123 95.2 98.4 78.0-123 3.31 20 7G1 Trichloroethene 0.125 0.140 0.141 112 113 76.0-126 0.712 20 Trichlorofluoromethane 0.125 0.152 0.145 122 116 61.0-142 4.71 20 1,2,3-Trichloropropane 0.125 0.125 0.126 100 101 67.0-129 0.797 20 FAI 1,2,3-Trim ethyl benzene 0.125 0.144 0.144 115 115 74.0-124 0.000 20 1,2,4-Trimethylbenzene 0.125 0.120 0.125 96.0 100 70.0-126 4.08 20 FSC 1,3,5-Trim ethyl benzene 0.125 0.120 0.126 96.0 101 73.0-127 4.88 20 Vinyl chloride 0.125 0.135 0.136 108 109 63.0-134 0.738 20 Xylenes,Total 0.375 0.379 0.383 101 102 72.0-127 1.05 20 (S)Toluene-d8 107 107 75.0-131 (S)4-Bromofluorobenzene 106 105 670-138 (S)1,2-Dich/oroethane-d4 104 105 70.0-130 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-Patriot Environmental Services MODESTO,CERES CA L1213730 05/05/20 19:35 37 of 56