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WG1470010 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 82606 L1213730-04 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) FP1(LCS)R3524524-1 05/04/2010:55•(LCSD)R3524524-2 05/04/2011:15 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits z Analyte mg/kg mg/kg mg/kg % % % % % TC Naphthalene 0.125 0.123 0.118 98.4 94.4 59.0-130 4.15 20 n-Propylbenzene 0.125 0.116 0.117 92.8 93.6 74.0-126 0.858 20 FSS Styrene 0.125 0.124 0.119 99.2 95.2 72.0-127 4.12 20 1,1,1,2-Tetrachloroethane 0.125 0.123 0.125 98.4 100 74.0-129 1.61 20 rCn 1,1,2,2-Tetrachloroethane 0.125 0.114 0.116 91.2 92.8 68.0-128 1.74 20 Tetrachloroethene 0.125 0.130 0.131 104 105 70.0-136 0.766 20 Toluene 0.125 0.116 0.113 92.8 90.4 75.0-121 2.62 20 FSr 1,1,2-Trichlorotrifluoroethane 0.125 0.162 0.158 130 126 61.0-139 2.50 20 1,2,3-Trichlorobenzene 0.125 0.132 0.123 106 98.4 59.0-139 7.06 20 1,2,4-Trichlorobenzene 0.125 0.137 0.128 110 102 62.0-137 6.79 20 1,1,1-Trichloroethane 0.125 0.132 0.131 106 105 69.0-126 0.760 20 1,1,2-Trichloroethane 0.125 0.120 0.115 96.0 92.0 78.0-123 4.26 20 7G1 Trichloroethene 0.125 0.132 0.134 106 107 76.0-126 1.50 20 Trichlorofluoromethane 0.125 0.151 0.142 121 114 61.0-142 6.14 20 1,2,3-Trichloropropane 0.125 0.125 0.127 100 102 67.0-129 1.59 20 FAI 1,2,3-Trim ethyl benzene 0.125 0.137 0.139 110 111 74.0-124 1.45 20 1,2,4-Trimethylbenzene 0.125 0.116 0.119 92.8 95.2 70.0-126 2.55 20 FSC 1,3,5-Trim ethyl benzene 0.125 0.115 0.115 92.0 92.0 73.0-127 0.000 20 Vinyl chloride 0.125 0.118 0.119 94.4 95.2 63.0-134 0.844 20 Xylenes,Total 0.375 0.360 0.359 96.0 95.7 72.0-127 0.278 20 (S)Toluene-d8 108 106 75.0-131 (S)4-Bromofluorobenzene 108 105 67.0-138 (S)1,2-Dich/oroethane-d4 105 105 70.0-130 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-Patriot Environmental Services MODESTO,CERES CA L1213730 05/05/20 19:35 41 of 56