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QC Sample Results <br />Client: Calgon Carbon Corporation Job ID: 180-113233-1 <br />Project/Site: Carbon Acceptance, 20201108.1 <br />Method: EPA 82700 - Semivolatile Organic Compounds (GC/MS) (Continued) <br />Lab Sample ID: LCS 180-336226/2-A <br />Matrix: Solid <br />Analysis Batch: 336270 <br />Analyte <br />Spike <br />Added <br />LCS LCS <br />Result Qualifier <br />Client Sample ID: Lab Control Sample <br />Prep Type: Total/NA <br />Prep Batch: 336226 <br />%Rec. <br />Unit D %Rec Limits <br />2,4-Dimethylphenol 100000 76700 ug/Kg 77 44 - 105 <br />Dimethyl phthalate 100000 75900 ug/Kg 76 49 - 111 <br />Di-n-butyl phthalate 100000 79900 ug/Kg 80 43 - 121 <br />4,6-Dinitro-2-methylphenol 200000 145000 ug/Kg 72 24 - 134 <br />2,4-Dinitrophenol 200000 98400 ug/Kg 49 10- 146 <br />2,4-Dinitrotoluene 100000 83300 ug/Kg 83 45 - 124 <br />2,6-Dinitrotoluene 100000 83500 ug/Kg 83 40 - 122 <br />Di-n-octyl phthalate 100000 63400 ug/Kg 63 33 - 129 <br />Fluoranthene 100000 78900 ug/Kg 79 40 - 120 <br />Fluorene 100000 78600 ug/Kg 79 46 - 109 <br />Hexachlorobenzene 100000 74500 ug/Kg 74 47 - 108 <br />Hexachlorobutadiene 100000 71700 ug/Kg 72 43 - 107 <br />Hexachlorocyclopentadiene 100000 64700 ug/Kg 65 23- 129 <br />Hexachloroethane 100000 86800 ug/Kg 87 35 - 104 <br />Indeno[1,2,3-cd]pyrene 100000 84200 ug/Kg 84 41 -125 <br />Isophorone 100000 73000 ug/Kg 73 40 - 110 <br />2-Methylnaphthalene 100000 82500 ug/Kg 82 45 - 100 <br />2-Methylphenol 100000 84600 ug/Kg 85 40 - 104 <br />Methylphenol, 3 & 4 100000 86200 ug/Kg 86 40 - 114 <br />Naphthalene 100000 76100 ug/Kg 76 38 - 105 <br />2-Nitroaniline 100000 73100 ug/Kg 73 45 - 117 <br />3-Nitroaniline 100000 77400 ug/Kg 77 34 - 122 <br />4-Nitroaniline 100000 76400 ug/Kg 76 38 - 123 <br />Nitrobenzene 100000 73300 ug/Kg 73 33 - 109 <br />2-Nitrophenol 100000 82600 ug/Kg 83 40 - 106 <br />4-Nitrophenol 200000 137000 ug/Kg 69 36 - 127 <br />N-Nitrosodi-n-propylamine 100000 85100 ug/Kg 85 42- 107 <br />N-Nitrosodiphenylamine 100000 78300 ug/Kg 78 44- 111 <br />2,2'-oxybis[1-chloropropane] 100000 70600 ug/Kg 71 31 -111 <br />Pentachlorophenol 200000 90100 ug/Kg 45 17- 122 <br />Phenanthrene 100000 76400 ug/Kg 76 43 _ 108 <br />Phenol 100000 81200 ug/Kg 81 41 - 102 <br />Pyrene 100000 76300 ug/Kg 76 41 - 115 <br />1,2,4-Trichlorobenzene 100000 75900 ug/Kg 76 43 - 100 <br />2,4,5-Trichlorophenol 100000 80400 ug/Kg 80 42- 112 <br />2,4,6-Trichlorophenol 100000 78600 ug/Kg 79 45 - 106 <br />LCS LCS <br />Surrogate %Recovery Qualifier Limits <br />2-Fluorobiphenyl 72 35-105 <br />2-Fluorophenol 79 39-103 <br />Nitrobenzene-d5 75 25-104 <br />Phenol-d5 83 25_105 <br />Terphenyl-d14 72 25-127 <br />2,4,6-Tribromophenol 74 35-124 <br />Eurofins TestAmerica, Pittsburgh <br />Page 15 of 20 11/11/2020