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1 12/20/17 12:30 12/21/1709:30 <br />0.1 35.9 <br />% 0.1 64.1 <br />Mercury <br />General Chemistry <br />Analyte <br />Percent Moisture <br />Percent Solids <br />0.064 <br />Result Qualifier <br />0.050 mg/Kg <br />RL Unit Prepared Analyzed Dil Fac <br />12/16/17 11:53 1 <br />12/16/17 11:53 1 <br />Client Sample Results <br />Client: Calgon Carbon Corporation <br />Project/Site: Carbon Acceptance, 20171212.1 <br />TestAmerica Job ID: 180-73514-7 <br />Client Sample ID: 20171212.1 <br />Date Collected: 12/15/17 00:00 <br />Date Received: 12/15/17 14:00 <br />Lab Sample ID: 180-73514-7 <br />Matrix: Solid <br />Percent Solids: 64.1 <br />Method: 8270C - Semivolatile Organic Compounds <br />Analyte Result Qualifier <br />4-Nitrophenol <br /> ND <br />N-Nitrosodi-n-propylamine ND <br />N-Nitrosodiphenylamine ND <br />2,2'-oxybis[1-chloropropane] <br /> ND <br />Pentachlorophenol ND <br />Phenanthrene ND <br />Phenol ND <br />Pyrene ND <br />1,2,4-Trichlorobenzene ND <br />2,4,5-Trichlorophenol ND <br />2,4,6-Trichlorophenol <br /> ND <br />(GC/MS) (Continued) <br />RL Unit <br /> <br />68000 ug/Kg <br /> <br />2700 ug/Kg <br /> <br />14000 ug/Kg <br /> <br />2700 ug/Kg <br /> <br />14000 ug/Kg <br /> <br />2700 ug/Kg <br /> <br />2700 ug/Kg <br /> <br />2700 ug/Kg <br /> <br />14000 ug/Kg <br /> <br />14000 ug/Kg <br /> <br />14000 ug/Kg <br />Prepared Analyzed Dil Fac <br />12/18/17 06:39 12/19/17 15:29 <br />12/18/17 06:39 12/19/17 15:29 <br />12/18/17 06:39 12/19/17 15:29 <br />12/18/17 06:39 12/19/17 15:29 <br />12/18/17 06:39 12/19/17 15:29 <br />12/18/17 06:39 12/19/17 15:29 <br />12/18/17 06:39 12/19/17 15:29 <br />12/18/17 06:39 12/19/17 15:29 <br />12/18/17 06:39 12/19/17 15:29 <br />12/18/17 06:39 12/19/17 15:29 <br />12/18/17 06:39 12/19/17 15:29 <br />Tentatively Identified Compound Est. Result Qualifier <br />Tentatively Identified Compound None <br />Surrogate %Recovery Qualifier <br />2-Fluorobiphenyl <br /> 64 <br />2-Fluorophenol 60 <br />Nitrobenzene-d5 80 <br />Phenol-d5 59 <br />Terphenyl-d14 45 <br />2,4,6-Tribromophenol 46 <br />Unit <br />ug/Kg <br />Limits <br />35- 105 <br />39-103 <br />25 - 104 <br />25 - 105 <br />25- 127 <br />35-124 <br />RT CAS No. Prepared Analyzed Dil Fac <br />Prepared Analyzed Dil Fac <br />12/18/1706.39 12/19/1715:29 1 <br />12/18/1706:39 12/19/1715.29 1 <br />12/18/1706.39 12/19/1715:29 1 <br />12/18/1706.39 12/19/17 15:29 1 <br />12/18/1706:39 12/19/17 15:29 1 <br />12/18/1706:39 12/19/1715:29 1 <br />12/18/17 06:39 12/19/17 15:29 <br /> <br />1 <br />Method: 6010B - Metals (ICP) <br />Analyte Result Qualifier RL Unit Prepared Analyzed Dil Fac <br />Lead ND 1.5 mg/Kg 0 12/18/17 13:09 12/19/17 14:33 1 <br />Method: 7471A - Mercury (CVAA) <br />Analyte Result Qualifier RL Unit Prepared Analyzed Dil Fac <br />TestAmerica Pittsburgh <br />Page 10 of 20 12/21/2017