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QC Sample Results <br />Client: Calgon Carbon Corporation TestAmerica Job ID: 180-66645-1 <br />Project/Site: Carbon Acceptance, 20170538.1 <br />Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) <br />Lab Sample ID: LCS 180-212391/2-A <br />Matrix: Solid <br />Analysis Batch: 212630 <br />Analyte <br />Spike <br />Added <br />LCS LCS <br />Result Qualifier <br />Client Sample ID: Lab Control Sample <br />Prep Type: Total/NA <br />Prep Batch: 212391 <br />%Rec. <br />Unit D %Rec Limits <br />Benzene 6250 5860 ug/Kg 94 77 - 120 <br />Chlorobenzene 6250 6020 ug/Kg 96 79 - 120 <br />1,1-Dichloroethene 6250 5270 ug/Kg 84 59 - 129 <br />Toluene 6250 6220 ug/Kg 100 78 - 124 <br />Trichloroethene 6250 5620 ug/Kg 90 76 - 119 <br />LCS LCS <br />Surrogate %Recovery Qualifier Limits <br />4-Bromofluorobenzene (Surr) 96 63 -120 <br />Dibromofluoromethane (Surr) 102 68- 121 <br />1,2-Dichloroethane-d4 (Surr) 97 52-124 <br />Toluene-d8 (Surr) 89 72- 127 <br />Lab Sample ID: LCSD 180-212391/3-A Client Sample ID: Lab Control Sample Dup <br />Matrix: Solid Prep Type: Total/NA <br />Analysis Batch: 212630 Prep Batch: 212391 <br />Analyte <br />Spike <br />Added <br />LCSD LCSD <br />Result Qualifier Unit D %Rec <br />%Rec. <br />Limits RPD <br />RPD <br />Limit <br />Benzene 6250 5890 ug/Kg 94 77 - 120 1 20 <br />Chlorobenzene 6250 6030 ug/Kg 97 79 - 120 0 20 <br />1,1-Dichloroethene 6250 4970 ug/Kg 80 59 - 129 6 25 <br />Toluene 6250 6330 ug/Kg 101 78 - 124 2 21 <br />Trichloroethene 6250 5770 ug/Kg 92 76 - 119 3 21 <br />LCSD LCSD <br />Surrogate %Recovery Qualifier Limits <br />4-Bromofluorobenzene (Surf) 100 63 -120 <br />Dibromofluoromethane (Surr) 100 68-121 <br />1,2-Dichloroethane-d4 (Surr) 102 52 -124 <br />Toluene-d8 (Surr) 93 72 -127 <br />Method: 8270C - Semivolatile Organic Compounds (GC/MS) <br />Lab Sample ID: MB 180-212676/1-A <br />Matrix: Solid <br />Analysis Batch: 212779 <br />Analyte <br />MB MB <br />Result Qualifier RL Unit <br />Client Sample ID: Method Blank <br />Prep Type: Total/NA <br />Prep Batch: 212676 <br />D Prepared Analyzed Dil Fac <br />Acenaphthene ND 2000 ug/Kg 05/30/17 12:20 05/31/17 12:31 1 <br />Acenaphthylene ND 2000 ug/Kg 05/30/17 12:20 05/31/17 12:31 1 <br />Anthracene ND 2000 ug/Kg 05/30/17 12:20 05/31/17 12:31 1 <br />Benzo[a]anthracene ND 2000 ug/Kg 05/30/17 12:20 05/31/17 12:31 1 <br />Benzo[a]pyrene ND 2000 ug/Kg 05/30/17 12:20 05/31/17 12:31 1 <br />Benzo[b]fluoranthene ND 2000 ug/Kg 05/30/17 12:20 05/31/17 12:31 1 <br />Benzo[g,h,i]perylene ND 2000 ug/Kg 05/30/17 12:20 05/31/17 12:31 1 <br />Benzo[k]fluoranthene ND 2000 ug/Kg 05/30/17 12:20 05/31/17 12:31 1 <br />Bis(2-chloroethoxy)methane ND 10000 ug/Kg 05/30/17 12:20 05/31/17 12:31 1 <br />Bis(2-chloroethyl)ether ND 2000 ug/Kg 05/30/17 12:20 05/31/17 12:31 1 <br />Bis(2-ethylhexyl) phthalate ND 20000 ug/Kg 05/30/17 12:20 05/31/17 12:31 1 <br />TestAmerica Pittsburgh <br />Page 12 of 22 6/2/2017