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Case Narrative <br />Client: Calgon Carbon Corporation TestAmerica Job ID: 180-88154-1 <br />Project/Site: Calgon Stockton Water <br />Job ID: 180-88154-1 <br /> <br />Laboratory: TestAmerica Pittsburgh <br />Narrative <br /> <br />Job Narrative <br />180-88154-1 <br />Receipt <br />The sample was received on 3/27/2019 10:10 AM; the sample arrived in good condition, properly preserved and, where required, on ice. <br />The temperature of the cooler at receipt was 1.7° C. <br />GC/MS VOA <br />Method(s) 8260B: The laboratory control sample (LCS) for analytical batch 720-262822 recovered above the control limits for the following <br />analyte: vinyl acetate. As this analyte was biased high in the LCS and was not detected in the associated sample; the results were <br />reported. <br />No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. <br />GC/MS Semi VOA <br />Method(s) 8270C: The following sample was diluted due to the abundance of non-target analytes: WASTE WATER (180-88154-1). <br />Elevated reporting limits (RLs) are provided. <br />Method(s) 8270C: The recovery of surrogates 2-fluorophenol and phenol-d5 was below the control limits for the following sample: WASTE <br />WATER (180-88154-1). Evidence of matrix interference is present; therefore, re-extraction and/or re-analysis was not performed. <br />Method(s) 8270C: The RPD between the laboratory control sample (LCS) and laboratory control sample duplicate (LCSD) for preparation <br />batch 720-262975 was above the control limits for pyridine. The recoveries were within the control limits. <br />No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. <br />Metals <br />Method(s) 6010B: Due to sample matrix effect on the internal standard (ISTD), a dilution was required for the following sample WASTE <br />WATER (180-88154-1). <br />No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. <br />TestAmerica Pittsburgh <br />4/3/2019 Page 3 of 30