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QC Sample Results <br />Client: Calgon Carbon Corporation TestAmerica Job ID: 180-88154-1 <br />Project/Site: Calgon Stockton Water <br />Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued) <br />Lab Sample ID: LCSD 720-262975/3-A <br />Matrix: Water <br />Analysis Batch: 263009 <br />Analyte <br />Spike <br />Added <br />LCSD LCSD <br />Result Qualifier <br />Client Sample ID: Lab Control Sample Dup <br />Prep Type: Total/NA <br />Prep Batch: 262975 <br />%Rec. RPD <br />Unit D %Rec Limits RPD Limit <br />Di-n-octyl phthalate 40.0 32.3 ug/L 81 70 - 115 2 35 <br />Fluoranthene 40.0 35.1 ug/L 88 65 _ 106 1 35 <br />Fluorene 40.0 31.0 ug/L 77 54 - 100 3 35 <br />Hexachlorobenzene 40.0 35.1 ug/L 88 60 - 100 1 35 <br />Hexachlorobutadiene 40.0 33.1 ug/L 83 40 - 110 4 35 <br />Hexachlorocyclopentadiene 40.0 16.8 ug/L 42 10 - 110 1 35 <br />Hexachloroethane 40.0 29.5 ug/L 74 34 - 110 1 35 <br />Indeno[1,2,3-cd]pyrene 40.0 35.4 ug/L 89 66 - 111 2 35 <br />Isophorone 40.0 30.2 ug/L 75 47 - 110 2 35 <br />2-Methyl-4,6-dinitrophenol 80.0 74.5 ug/L 93 42 - 121 0 35 <br />2-Methylnaphthalene 40.0 31.4 ug/L 78 44 - 110 2 35 <br />2-Methylphenol 40.0 24.3 ug/L 61 34 - 110 4 35 <br />Methylphenol, 3 & 4 40.0 23.3 ug/L 58 31 _ 110 3 35 <br />Naphthalene 40.0 30.8 ug/L 77 41 - 110 2 35 <br />2-Nitroaniline 40.0 31.0 ug/L 78 55 - 105 1 35 <br />3-Nitroaniline 40.0 26.3 ug/L 66 56 - 110 1 35 <br />4-Nitroaniline 40.0 29.2 ug/L 73 57 - 105 0 35 <br />Nitrobenzene 40.0 28.1 ug/L 70 41 - 110 0 35 <br />2-Nitrophen0l 40.0 34.1 ug/L 85 40 _ 100 0 35 <br />4-Nitrophenol 80.0 24.3 ug/L 30 15 - 110 5 35 <br />N-Nitrosodi-n-propylamine 40.0 25.8 ug/L 64 42 - 110 0 35 <br />N-Nitrosodiphenylamine 40.0 33.1 ug/L 83 60 - 100 1 35 <br />Pentachlorophenol 80.0 66.8 ug/L 84 54 _ 105 2 35 <br />Phenanthrene 40.0 33.5 ug/L 84 62 - 102 1 35 <br />Phenol 40.0 10.8 ug/L 27 10 - 110 8 35 <br />Pyrene 40.0 34.9 ug/L 87 68 - 115 2 35 <br />Pyridine 80.0 19.4 ug/L 24 10 - 49 66 35 <br />1,2,4-Trichlorobenzene 40.0 30.7 ug/L 77 40 - 110 2 35 <br />2,4,5-Trichlorophenol 40.0 31.8 ug/L 79 53 - 101 2 35 <br />2,4,6-Trichlorophenol 40.0 30.9 ug/L 77 50 _ 100 0 35 <br />LCSD LCSD <br />Surrogate %Recovery Qualifier Limits <br />2-Fluorobiphenyl 73 10- 101 <br />2-Fluorophenol 38 10- 65 <br />Nitrobenzene-d5 66 11 -92 <br />Phenol-d5 26 10 - 46 <br />Terphenyl-d14 97 34 - 128 <br />2,4,6-Tribromophenot 90 17 _ 115 <br />Method: 6010B - Metals (ICP) <br />Lab Sample ID: MB 720-262772/1-A <br /> Client Sample ID: Method Blank <br />Matrix: Water Prep Type: Total/NA <br />Analysis Batch: 262935 <br /> Prep Batch: 262772 <br />MB MB <br />Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac <br />Antimony ND 0.010 mg/L 03/28/19 09:41 03/29/19 17:25 1 <br />Arsenic ND 0.010 mg/L 03/28/19 09:41 03/29/19 17:25 1 <br />TestAnnerica Pittsburgh <br />Page 22 of 30 4/3/2019