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Lab Sample ID: LCSI 180-212622/3-A <br />Matrix: Solid <br />Analysis Batch: 212790 <br />Analyte <br />Spike <br />Added <br /> <br />LCSI LCSI <br /> <br />Result Qualifier <br />Client Sample ID: Lab Control Sample <br />Prep Type: Total/NA <br />Prep Batch: 212622 <br />%Rec. <br />Unit D %Rec Limits <br />Hexavalent chromium 708 687 mg/Kg 97 80 - 120 <br />Lab Sample ID: LCSS 180-212622/2-A Client Sample ID: Lab Control Sample <br />Matrix: Solid Prep Type: Total/NA <br />Analysis Batch: 212790 Prep Batch: 212622 <br />Spike LCSS LCSS %Rec. <br />Analyte Added Result Qualifier Unit D %Rec Limits <br />Hexavalent chromium 20.0 17.6 mg/Kg 88 80 - 120 <br />Lab Sample ID: 180-66645-2 MSI Client Sample ID: 20170538.2 <br />Matrix: Solid Prep Type: Total/NA <br />Analysis Batch: 212790 Prep Batch: 212622 <br />Sample Sample Spike MSI MSI %Rec. <br />Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br />Hexavalent chromium ND Fl 1320 981 Fl mg/Kg <, 74 75 - 125 <br />Lab Sample ID: 180-66645-2 MSS Client Sample ID: 20170538.2 <br />Matrix: Solid Prep Type: Total/NA <br />Analysis Batch: 212790 Prep Batch: 212622 <br />Sample Sample Spike MSS MSS %Rec. <br />Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br />Hexavalent chromium ND Fl 38.1 0.798 Fl mg/Kg 2 75 - 125 <br />Lab Sample ID: 180-66645-2 DU Client Sample ID: 20170538.2 <br />Matrix: Solid Prep Type: Total/NA <br />Analysis Batch: 212790 Prep Batch: 212622 <br />Sample Sample DU DU RPD <br />Analyte Result Qualifier Result Qualifier Unit RPD Limit <br />Hexavalent chromium ND Fl ND mg/Kg NC 20 <br />Lab Sample ID: MB 180-212625/1-A <br />Matrix: Solid <br />Analysis Batch: 212939 <br />Client Sample ID: Method Blank <br />Prep Type: Total/NA <br />Prep Batch: 212625 <br />MB MB <br />Analyte Result Qualifier RL Unit D Prepared Analyzed Oil Fac <br />Hexavalent chromium ND <br /> <br />0.40 mg/Kg 05/30/17 07:00 05/31/17 12:58 1 <br />Lab Sample ID: LCSI 180-212625/3-A <br />Matrix: Solid <br />Analysis Batch: 212939 <br />Analyte <br />Spike <br />Added <br />LCSI LCSI <br />Result Qualifier <br />Client Sample ID: Lab Control Sample <br />Prep Type: Total/NA <br />Prep Batch: 212625 <br />%Rec. <br />Unit D %Rec Limits <br />Hexavalent chromium 708 692 mg/Kg 98 80 - 120 <br />Lab Sample ID: LCSS 180-212625/2-A Client Sample ID: Lab Control Sample <br />Matrix: Solid Prep Type: Total/NA <br />Analysis Batch: 212939 Prep Batch: 212625 <br />Spike LCSS LCSS %Rec. <br />Analyte Added Result Qualifier Unit D %Rec Limits <br />Hexavalent chromium 20.0 17.5 mg/Kg 88 80 - 120 <br />QC Sample Results <br />Client: Calgon Carbon Corporation <br />Project/Site: Carbon Acceptance, 20170538.2 <br /> <br />TestAmerica Job ID: 180-66645-2 <br />Method: 7196A - Chromium, Hexavalent (Continued) <br /> <br />TestAmerica Pittsburgh <br />Page 10 of 15 6/2/2017