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QC Sample Results <br />Client: Calgon Carbon Corporation TestAmerica Job ID: 180-80873-5 <br />Project/Site: Carbon Acceptance, 20180818.1 <br />Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued) <br />Lab Sample ID: LCS 180-254120/2-A <br />Matrix: Solid <br />Analysis Batch: 254038 <br />Analyte <br />Spike <br />Added <br />LCS LCS <br />Result Qualifier <br />Client Sample ID: Lab Control Sample <br />Prep Type: Total/NA <br />Prep Batch: 254120 <br />%Rec. <br />Unit D %Rec Limits <br />Benzene 6250 4780 ug/Kg 77 74 - 117 <br />Chlorobenzene 6250 5860 ug/Kg 94 77 - 117 <br />1,1-Dichloroethene 6250 4040 ug/Kg 65 62 - 127 <br />Toluene 6250 5290 ug/Kg 85 73 - 122 <br />Trichloroethene 6250 5180 ug/Kg 83 75 - 121 <br />LCS LCS <br />Surrogate %Recovery Qualifier Limits <br />4-Bromofluorobenzene (Surr) 81 60127 <br />Dibromofluoromethane (Surr) 86 70 _ 121 <br />1,2-Dichloroethane-d4 (Surr) 86 52-135 <br />Toluene-d8 (Surf) 97 72-123 <br />Lab Sample ID: LCSD 180-254120/3-A <br /> Client Sample ID: Lab Control Sample Dup <br />Matrix: Solid <br /> Prep Type: Total/NA <br />Analysis Batch: 254038 <br /> Prep Batch: 254120 <br />Analyte <br />Spike <br />Added <br />LCSD LCSD <br />Result Qualifier Unit D %Rec <br />%Rec. <br />Limits RPD <br />RPD <br />Limit <br />Benzene 6250 4630 ug/Kg 74 74- 117 3 15 <br />Chlorobenzene 6250 5780 ug/Kg 92 77 - 117 1 15 <br />1,1-Dichloroethene 6250 3990 ug/Kg 64 62 - 127 1 19 <br />Toluene 6250 5180 ug/Kg 83 73 - 122 2 15 <br />Trichloroethene 6250 5020 ug/Kg 80 75 - 121 3 15 <br />LCSD LCSD <br />Surrogate %Recovery Qualifier Limits <br />4-Bromofluorobenzene (Surr) 81 60 -127 <br />Dibromofluoromethane (Sun-) 86 70 -121 <br />1,2-Dichloroethane-d4 (Surr) 86 52- 135 <br />Toluene-d8 (Surr) 98 72 -123 <br />Method: EPA 8270C - Semivolatile Organic Compounds (GC/MS) <br />Lab Sample ID: MB 180-253964/1-A <br />Matrix: Solid <br />Analysis Batch: 254092 <br />Analyte <br />MB MB <br />Result Qualifier RL Unit <br />Client Sample ID: Method Blank <br />Prep Type: Total/NA <br />Prep Batch: 253964 <br />D Prepared Analyzed Oil Fac <br />Acenaphthene ND 2000 ug/Kg 08/15/18 12:08 08/16/18 12:05 1 <br />Acenaphthylene ND 2000 ug/Kg 08/15/18 12:08 08/16/18 12:05 1 <br />Anthracene ND 2000 ug/Kg 08/15/18 12:08 08/16/18 12:05 1 <br />Benzo[a]anthracene ND 2000 ug/Kg 08/15/18 12:08 08/16/18 12:05 1 <br />Benzolalpyrene ND 2000 ug/Kg 08/15/18 12:08 08/16/18 12:05 1 <br />Benzo[b]fluoranthene ND 2000 ug/Kg 08/15/18 12:08 08/16/18 12:05 1 <br />Benzo[g,h,i]perylene ND 2000 ug/Kg 08/15/18 12:08 08/16/18 12:05 1 <br />Benzo[k]fluoranthene ND 2000 ug/Kg 08/15/18 12:08 08/16/18 12:05 1 <br />Bis(2-chloroethoxy)methane ND 10000 ug/Kg 08/15/18 12:08 08/16/18 12:05 1 <br />Bis(2-chloroethyl)ether ND 2000 ug/Kg 08/15/18 12:08 08/16/18 12:05 1 <br />Bis(2-ethylhexyl) phthalate ND 20000 ug/Kg 08/15/18 12:08 08/16/18 12:05 1 <br />TestAmerica Pittsburgh <br />Page 12 of 20 8/20/2018