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Client Sample ID: Method Blank <br />Prep Type: Total/NA <br />Prep Batch: 253964 <br />Lab Sample ID: MB 180-253964/1-A <br />Matrix: Solid <br />Analysis Batch: 254092 <br />Unit RL <br />ug/Kg <br />ug/Kg <br />ug/Kg <br />ug/Kg <br />ug/Kg <br />2000 <br />2000 <br />10000 <br />10000 <br />10000 <br />Analyte <br />Phenol <br />MB MB <br />Result Qualifier <br />ND <br />ND <br />ND <br />ND <br />ND <br />D Prepared <br />08/15/18 12:08 <br />08/15/18 12:08 <br />08/15/18 12:08 <br />08/15/18 12:08 <br />08/15/18 12:08 <br />Pyrene <br />1,2,4-Trichlorobenzene <br />2,4,5-Trichlorophenol <br />2,4,6-Trichlorophenol <br />Analyzed Dil Fac <br />08/16/18 12:05 1 <br />08/16/18 12:05 1 <br />08/16/18 12:05 1 <br />08/16/18 12:05 1 <br />08/16/18 12:05 1 <br />Analyzed Dil Fac RT CAS No. Prepared <br />Surrogate <br />08/15/18 12:08 <br />08/15/18 12:08 <br />08/15/18 12:08 <br />08/15/18 12:08 <br />08/15/18 12:08 <br />08/15/18 12:08 <br />Prepared <br />2-Fluorobiphenyl <br />2-Fluorophenol <br />Nitrobenzene-d5 <br />Phenol-d5 <br />Terphenyl-d14 <br />2,4,6-Tribromophenol <br />Analyzed Dil Fac <br />08/16/18 12:05 1 <br />08/16/18 12:05 1 <br />08/16/18 12:05 1 <br />08/16/18 12.05 1 <br />08/16/18 12.05 1 <br />08/16/18 12:05 1 <br />MB MB <br />%Recovery Qualifier Limits <br />64 35105 <br />72 39-103 <br />67 25 - 104 <br />67 25 - 105 <br />67 25 _ 127 <br />71 35-124 <br />MB MB <br />Tentatively Identified Compound Est. Result Qualifier Unit <br />Tentatively Identified Compound None ug/Kg 08/15/18 12:08 08/16/18 12:05 1 <br />Lab Sample ID: LCS 180-253964/2-A <br />Matrix: Solid <br />Analysis Batch: 254092 <br />Analyte <br />Spike <br />Added <br />LCS LCS <br />Result Qualifier <br />Client Sample ID: Lab Control Sample <br />Prep Type: Total/NA <br />Prep Batch: 253964 <br />%Rec. <br />Unit D %Rec Limits <br />Acenaphthene 100000 69800 ug/Kg 70 47 - 104 <br />Acenaphthylene 100000 69000 ug/Kg 69 49 - 114 <br />Anthracene 100000 65300 ug/Kg 65 45 - 112 <br />Benzo[alanthracene 100000 61800 ug/Kg 62 47 - 110 <br />Benzo[a]pyrene 100000 57600 ug/Kg 58 40 _ 112 <br />Benzo[b]fluoranthene 100000 55900 ug/Kg 56 41 - 107 <br />Benzo[g,h,i]perylene 100000 66700 ug/Kg 67 38 - 126 <br />Benzo[k]fluoranthene 100000 57900 ug/Kg 58 40 - 115 <br />Bis(2-chloroethoxy)methane 100000 66700 ug/Kg 67 38 - 105 <br />Bis(2-chloroethyl)ether 100000 70500 ug/Kg 71 35 - 106 <br />Bis(2-ethylhexyl) phthalate 100000 70200 ug/Kg 70 40 - 117 <br />4-Bromophenyl phenyl ether 100000 62000 ug/Kg 62 47 - 110 <br />Butyl benzyl phthalate 100000 70500 ug/Kg 71 35 _ 118 <br />Carbazole 100000 71000 ug/Kg 71 45 _ 114 <br />4-Chloroaniline 100000 63800 ug/Kg 64 25 - 108 <br />4-Chloro-3-methylphenol 100000 66600 ug/Kg 67 40 - 109 <br />2-Chloronaphthalene 100000 66300 ug/Kg 66 46 _ 101 <br />2-Chlorophenol 100000 71600 ug/Kg 72 40 _ 101 <br />4-Chlorophenyl phenyl ether 100000 62200 ug/Kg 62 47 - 109 <br />Chrysene 100000 58700 ug/Kg 59 46 _ 111 <br />Dibenz(a,h)anthracene 100000 60900 ug/Kg 61 39 - 127 <br />Dibenzofuran 100000 68900 ug/Kg 69 46 - 104 <br />1,2-Dichlorobenzene 100000 64100 ug/Kg 64 36 - 101 <br />1,3-Dichlorobenzene 100000 64100 ug/Kg 64 35 - 101 <br />1,4-Dichlorobenzene 100000 63500 ug/Kg 63 36 - 101 <br />QC Sample Results <br />Client: Calgon Carbon Corporation TestAmerica Job ID: 180-80873-5 <br />Project/Site: Carbon Acceptance, 20180818.1 <br />Method: EPA 8270C - Semivolatile Organic Compounds (GC/MS) (Continued) <br />TestAmerica Pittsburgh <br />Page 14 of 20 8/20/2018