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QC Sample Results <br />Client: Calgon Carbon Corporation TestAmerica Job ID: 180-80873-6 <br />Project/Site: Carbon Acceptance, 20180818.2 <br />Method: EPA 6010B - Metals (ICP) <br />Lab Sample ID: MB 180-254171/1-A <br />Matrix: Solid <br />Analysis Batch: 254401 <br />Analyte <br />MB MB <br />Result Qualifier RL Unit <br />Client Sample ID: Method Blank <br />Prep Type: Total/NA <br />Prep Batch: 254171 <br />D Prepared Analyzed Dil Fac <br />Antimony ND 1.0 mg/Kg 08/16/18 18:14 08/20/18 08:13 1 <br />Arsenic ND 1.0 mg/Kg 08/16/18 18:14 08/20/18 08:13 1 <br />Barium ND 20 mg/Kg 08/16/18 18:14 08/20/18 08:13 1 <br />Beryllium ND 0.40 mg/Kg 08/16/18 18:14 08/20/18 08:13 1 <br />Cadmium ND 0.50 mg/Kg 08/16/18 18:14 08/20/18 08:13 1 <br />Calcium ND 500 mg/Kg 08/16/18 18:14 08/20/18 08:13 1 <br />Chromium ND 0.50 mg/Kg 08/16/18 18:14 08/20/18 08:13 1 <br />Cobalt ND 5.0 mg/Kg 08/16/18 18:14 08/20/18 08:13 1 <br />Copper ND 2.5 mg/Kg 08/16/18 18:14 08/20/18 08:13 1 <br />Iron ND 10 mg/Kg 08/16/18 18:14 08/20/18 08:13 1 <br />Manganese ND 1.5 mg/Kg 08/16/18 18:14 08/20/18 08:13 1 <br />Nickel ND 4.0 mg/Kg 08/16/18 18:14 08/20/18 08:13 1 <br />Selenium ND 1.0 mg/Kg 08/16/18 18:14 08/20/18 08:13 1 <br />Silver ND 0.50 mg/Kg 08/16/18 18:14 08/20/18 08:13 1 <br />Thallium ND 2.0 mg/Kg 08/16/18 18:14 08/20/18 08:13 1 <br />Zinc ND 2.0 mg/Kg 08/16/18 18:14 08/20/18 08:13 1 <br />Lab Sample ID: LCS 180-254171/2-A <br />Matrix: Solid <br />Analysis Batch: 254401 <br />Analyte <br />Spike <br />Added <br />LCS LCS <br />Result Qualifier <br />Client Sample ID: Lab Control Sample <br />Prep Type: Total/NA <br />Prep Batch: 254171 <br />%Rec. <br />Unit D %Rec Limits <br />Antimony 50.0 50.5 mg/Kg 101 80 _ 120 <br />Arsenic 50.0 49.3 mg/Kg 99 80 - 120 <br />Barium 200 203 mg/Kg 102 80 - 120 <br />Beryllium 5.00 4.92 mg/Kg 98 80 - 120 <br />Cadmium 5.00 4.96 mg/Kg 99 80-120 <br />Calcium 5000 4690 mg/Kg 94 80 - 120 <br />Chromium 20.0 19.9 mg/Kg 100 80 - 120 <br />Cobalt 50.0 50.3 mg/Kg 101 80 - 120 <br />Copper 25.0 25.0 mg/Kg 100 80 - 120 <br />Iron 100 98.7 mg/Kg 99 80 _ 120 <br />Manganese 50.0 48.8 mg/Kg 98 80 - 120 <br />Nickel 50.0 50.3 mg/Kg 101 80 - 120 <br />Selenium 50.0 51.1 mg/Kg 102 80 - 120 <br />Silver 5.00 5.15 mg/Kg 103 80 - 120 <br />Thallium 50.0 48.5 mg/Kg 97 80 - 120 <br />Zinc 50.0 49.7 mg/Kg 99 80 - 120 <br />Method: EPA 7196A - Chromium, Hexavalent <br />Lab Sample ID: MB 180-253822/1-A <br />Matrix: Solid <br />Analysis Batch: 254192 <br />Client Sample ID: Method Blank <br />Prep Type: Total/NA <br />Prep Batch: 253822 <br />MB MB <br />Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac <br />Hexavalent chromium ND 0.40 mg/Kg 08/14/18 14:58 08/17/18 08:40 1 <br />TestAmerica Pittsburgh <br />Page 9 of 13 8/20/2018