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QC Sample Results <br />Client: Calgon Carbon Corporation TestAmerica Job ID: 180-81562-5 <br />Project/Site: Carbon Acceptance, 20180852.1 <br />Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued) <br />pLab Sample ID: LCS 180-255984/2-A <br />Matrix: Solid <br />Analysis Batch: 255876 <br />Analyte <br />Spike <br />Added <br />LCS LCS <br />Result Qualifier <br />Client Sample ID: Lab Control Sample <br />Prep Type: Total/NA <br />Prep Batch: 255984 <br />%Rec. <br />Unit D %Rec Limits <br />Benzene 6250 4880 ug/Kg 78 76 - 116 <br />Chlorobenzene 6250 5910 ug/Kg 95 78 _ 118 <br />1,1-Dichloroethene 6250 4310 ug/Kg 69 57 - 131 <br />Toluene 6250 5370 ug/Kg 86 76 _ 126 <br />Trichloroethene 6250 5120 ug/Kg 82 70 - 121 <br />LCS LCS <br />Surrogate %Recovery Qualifier Limits <br />4-Bromofluorobenzene (Surr) 82 60_127 <br />Dibromofluoromethane (Surr) 90 70 -121 <br />1,2-Dichloroethane-d4 (Surr) 87 52 -135 <br />Toluene-d8 (Surr) 99 72- 123 <br />Lab Sample ID: LCSD 180-255984/3-A <br />Matrix: Solid <br />Analysis Batch: 255876 <br />Client Sample ID: Lab Control Sample Dup <br />Prep Type: Total/NA <br />Prep Batch: 255984 <br />Analyte <br />Spike <br />Added <br />LCSD LCSD <br />Result Qualifier Unit D %Rec <br />%Rec. <br />Limits RPD <br />RPD <br />Limit <br />Benzene 6250 4740 ug/Kg 76 76 - 116 3 20 <br />Chlorobenzene 6250 5800 ug/Kg 93 78- 118 2 20 <br />1,1-Dichloroethene 6250 3960 ug/Kg 63 57 - 131 8 20 <br />Toluene 6250 5190 ug/Kg 83 76 - 126 4 20 <br />Trichloroethene 6250 4980 ug/Kg 80 70 _ 121 3 20 <br />LCSD LCSD <br />Surrogate %Recovery Qualifier Limits <br />4-Bromofluorobenzene (Surr) 80 60- 127 <br />Dibromofluoromethane (Surr) 86 70 -121 <br />1,2-Dichloroethane-d4 (Surr) 85 52- /35 <br />Toluene-d8 (Surr) 98 72-123 <br />Method: EPA 8270C - Semivolatile Organic Compounds (GC/MS) <br />Lab Sample ID: MB 180-256235/1-A <br />Matrix: Solid <br />Analysis Batch: 256279 <br />Analyte <br />MB MB <br />Result Qualifier RL Unit <br />Client Sample ID: Method Blank <br />Prep Type: Total/NA <br />Prep Batch: 256235 <br />D Prepared Analyzed Dil Fac <br />Acenaphthene ND 2000 ug/Kg 09/07/18 15:02 09/08/18 13:07 1 <br />Acenaphthylene ND 2000 ug/Kg 09/07/18 15:02 09/08/18 13:07 1 <br />Anthracene ND 2000 ug/Kg 09/07/18 15:02 09/08/18 13:07 1 <br />Benzo[a]anthracene ND 2000 ug/Kg 09/07/18 15:02 09/08/18 13:07 1 <br />Benzo[a]pyrene ND 2000 ug/Kg 09/07/18 15:02 09/08/18 13:07 1 <br />Benzo[b]fluoranthene ND 2000 ug/Kg 09/07/18 15:02 09/08/18 13:07 1 <br />Benzolg,h,ilperylene ND 2000 ug/Kg 09/07/18 15:02 09/08/18 13:07 1 <br />Benzo[k]fluoranthene ND 2000 ug/Kg 09/07/18 15:02 09/08/18 13:07 1 <br />Bis(2-chloroethoxy)methane ND 10000 ug/Kg 09/07/18 15:02 09/08/18 13:07 1 <br />Bis(2-chloroethyl)ether ND 2000 ug/Kg 09/07/18 15:02 09/08/18 13:07 1 <br />Bis(2-ethylhexyl) phthalate ND 20000 ug/Kg 09/07/18 15:02 09/08/18 13:07 1 <br />TestAmerica Pittsburgh <br />Page 12 of 20 9/11/2018 <br />LI Ei <br />9