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MB MB <br />Result Qualifier Analyte <br />9 DII Fac RT CAS No. Prepared Analyzed <br />MB MB <br />Tentatively Identified Compound Est. Result Qualifier Unit <br />1 None ug/Kg 09/07/18 15:02 09/08/18 13:07 Tentatively Identified Compound <br />MB MB <br />%Recovery Qualifier Limits Prepared Analyzed Dil Fac Surrogate <br />Lab Sample ID: MB 180-256235/1-A <br />Matrix: Solid <br />Analysis Batch: 256279 <br />Phenol <br />Pyrene <br />1,2,4-Trichlorobenzene <br />2,4,5-Trichlorophenol <br />2,4,6-Trichlorophenol <br />Client Sample ID: Method Blank 121 <br />Prep Type: Total/NA <br />Prep Batch: 256235 Ei <br />RL Unit D Prepared Analyzed Dil Fac <br />2000 ug/Kg 09/07/18 15:02 09/08/18 13:07 1 <br />2000 ug/Kg 09/07/18 15:02 09/08/18 13:07 1 <br />10000 ug/Kg 09/07/18 15:02 09/08/18 13:07 1 <br />10000 ug/Kg 09/07/18 15:02 09/08/18 13:07 1 <br />10000 ug/Kg 09/07/18 15:02 09/08/18 13:07 1 <br />ND <br />ND <br />ND <br />ND <br />ND <br />2-Fluorobiphenyl <br />2-Fluorophenol <br />Nitrobenzene-d5 <br />Phenol-d5 <br />Terphenyl-d14 <br />2,4,6-Tribromophenol <br />74 35105 09/07/18 15:02 09/08/18 13.'07 <br />76 39103 09/07/18 15:02 09/08/18 13:07 <br />76 25 -104 09/07/18 15:02 09/08/18 13:07 <br />81 25 -105 09/07/18 15:02 09/08/18 13:07 <br />82 25 _127 09/07/18 15:02 09/08/18 13:07 <br />65 35-124 09/07/18 15:02 09/08/18 13:07 <br />Lab Sample ID: LCS 180-256235/2-A <br />Matrix: Solid <br />Analysis Batch: 256279 <br />Analyte <br />Spike <br />Added <br />LCS LCS <br />Result Qualifier <br />Client Sample ID: <br />Unit D %Rec <br />Lab Control Sample <br />Prep Type: Total/NA <br />Prep Batch: 256235 <br />%Rec. <br />Limits <br />Acenaphthene 100000 91200 ug/Kg 91 47 - 104 <br />Acenaphthylene 100000 88200 ug/Kg 88 49 - 114 <br />Anthracene 100000 95600 ug/Kg 96 45 - 112 <br />Benzo[a]anthracene 100000 87200 ug/Kg 87 47 - 110 <br />Benzo[a]pyrene 100000 92500 ug/Kg 93 40 - 112 <br />Benzo[b]fluoranthene 100000 80500 ug/Kg 81 41 -107 <br />Benzo[g,h,i]perylene 100000 91300 ug/Kg 91 38 - 126 <br />Benzo[k]fluoranthene 100000 89600 ug/Kg 90 40 - 115 <br />Bis(2-chloroethoxy)methane 100000 77200 ug/Kg 77 38 - 105 <br />Bis(2-chloroethyl)ether 100000 81300 ug/Kg 81 35 - 106 <br />Bis(2-ethylhexyl) phthalate 100000 95500 ug/Kg 96 40 - 117 <br />4-Bromophenyl phenyl ether 1 00000 83500 ug/Kg 84 47 - 110 <br />Butyl benzyl phthalate 100000 93800 ug/Kg 94 35 _ 118 <br />Carbazole 100000 96300 ug/Kg 96 45 - 114 <br />4-Chloroaniline 100000 82600 ug/Kg 83 25 - 108 <br />4-Chloro-3-methylphenol 100000 74800 ug/Kg 75 40 - 109 <br />2-Chloronaphthalene 100000 90500 ug/Kg 90 46 - 101 <br />2-Chlorophenol 100000 85500 ug/Kg 85 40- 101 <br />4-Chlorophenyl phenyl ether 100000 79100 ug/Kg 79 47 - 109 <br />Chrysene 100000 86500 ug/Kg 86 46- 111 <br />Dibenz(a,h)anthracene 100000 89600 ug/Kg 90 39 - 127 <br />Dibenzofuran 100000 89900 ug/Kg 90 46- 104 <br />1,2-Dichlorobenzene 100000 87000 ug/Kg 87 36 - 101 <br />1,3-Dichlorobenzene 100000 87900 ug/Kg 88 35 - 101 <br />1,4-Dichlorobenzene 100000 87500 ug/Kg 88 36 - 101 <br />QC Sample Results <br />Client: Calgon Carbon Corporation <br />TestAmerica Job ID: 180-81562-5 <br />Project/Site: Carbon Acceptance, 20180852.1 <br />Method: EPA 8270C - Semivolatile Organic Compounds (GC/MS) (Continued) <br />TestAmerica Pittsburgh <br />Page 14 of 20 9/11/2018