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Quality Control Report <br />McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 <br />http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts" <br />Client:AdvancedGeo, Inc. <br />Project:Pilkington <br />Date Analyzed:02/03/2021 <br />Date Prepared:02/02/2021 <br />WorkOrder:2102062 <br />BatchID:214296 <br />Analytical Method:SW8082 <br />Unit:mg/kg <br />Sample ID:MB/LCS/LCSD-214296 <br />2102062-003AMS/MSD <br />Instrument:GC40 <br />Matrix:Soil <br />Extraction Method:SW3550B <br />QC Summary Report for SW8082 <br />Analyte MB <br />Result <br />MDL RL SPK <br />Val <br />MB SS <br />%REC <br />MB SS <br />Limits <br />Aroclor1016 ND 0.00510 0.0500 --- <br />Aroclor1221 ND 0.0110 0.0500 --- <br />Aroclor1232 ND 0.00630 0.0500 --- <br />Aroclor1242 ND 0.00670 0.0500 --- <br />Aroclor1248 ND 0.00400 0.0500 --- <br />Aroclor1254 ND 0.00680 0.0500 --- <br />Aroclor1260 ND 0.00610 0.0500 --- <br />Surrogate Recovery <br />Decachlorobiphenyl 0.0486 0.05 97 70-130 <br />Analyte LCS <br />Result <br />LCSD <br />Result <br />SPK <br />Val <br />LCS <br />%REC <br />LCSD <br />%REC <br />LCS/LCSD <br />Limits <br />RPD RPD <br />Limit <br />Aroclor1016 0.148 0.150 0.15 99 100 70-130 0.888 20 <br />Aroclor1260 0.142 0.148 0.15 95 99 70-130 3.81 20 <br />Surrogate Recovery <br />Decachlorobiphenyl 0.0467 0.0489 0.050 93 98 70-130 4.73 20 <br />Analyte MS <br />Result <br />MSD <br />Result <br />SPK <br />Val <br />SPKRef <br />Val <br />MS <br />%REC <br />MSD <br />%REC <br />MS/MSD <br /> Limits <br />RPD RPD <br />Limit <br />MS <br />DF <br />Aroclor1016 0.149 0.151 0.15 ND 99 101 60-130 1.74 201 <br />Aroclor1260 0.132 0.132 0.15 ND 88 88 60-130 0.745 201 <br />Surrogate Recovery <br />Decachlorobiphenyl 0.0415 0.0404 0.0501 83 81 60-130 2.76 20 <br />CA ELAP 1644 • NELAP 4033ORELAP <br />Page 111 of 154