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CLIENT: <br />PRUF11 <br />E <br />kip] <br />WORLD ENTERPRISEZ� <br />061291 <br />E <br />METHOD 603013/826013 <br />VOLATILE ORGANICS BY GC/MS <br />Three (3) water samples were received on 09/30/06 for Volatile Organic analysis by <br />Method 5030B/8260B in accordance with DDJC-Sharpe[Tracy QAPP. <br />1. Holding Time <br />Analytical holding time was met. <br />2. Tuning and Calibration <br />Tuning and calibration were carried out at 12 -hour interval, All QC requirements <br />were met. <br />3. Method Blank <br />Method blank was free of contamination at the reporting limit. <br />4. Surrogate Recovery <br />Recoveries were within QC limit. <br />6. Lab Control Sample/Lab Control Sample Duplicate <br />Recoveries were within QC limit. <br />6. Matrix Spike/Matrix Spike Duplicate <br />No MS/MSD sample was designated in this SDG. <br />7. Sample Analysis <br />Samples were analyzed according to the prescribed QC procedures. All criteria <br />were met. <br />M M 4 <br />