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1534 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> M c C am p b e I l Analytical, Inc. Toll Free Telephone:(877)252-9262/Fax:(925)252-9269 <br /> "When Quality Counts" I <br /> http://www.mccanTbell.com/E-mail:main@mccampbell.com <br /> Analytical Report <br /> Client: BSK Associates Engineers&Laboratories WorkOrder: 2406880 <br /> Date Received: 06/13/2024 12:30 Extraction Method: DOD QSM <br /> Date Prepared: 06/18/2024 Analytical Method: DOD QSM <br /> Project: E2001601F.004.002; SCK Unit: µg/Kg <br /> Perfluorinated Compounds <br /> Client ID Lab ID Matrix Date Collected instrument Batch ID <br /> B-21 V 2406880-012A Soil 06/11/2024 13:28 LC-MS3 06202024 DOD S_ 295928 <br /> Analytes Result MDL RL DF Date Analyzed <br /> P FOSA ND 0.21 1.0 1 06/20/2024 16:41 <br /> PFPeA ND 0.26 1.0 1 06/20/2024 16:41 <br /> PFPeS ND 0.17 1.0 1 06/20/2024 16:41 <br /> PFTeDA ND 0.19 1.0 1 06/20/2024 16:41 <br /> PFTrDA ND 0.29 1.0 1 06/20/2024 16:41 <br /> PFUnA ND 0.34 1.0 1 06/20/2024 16:41 <br /> Internal Standard REC % Limits <br /> 13C2-4:2 FTS 97 50-150 1 06/20/2024 16:41 <br /> 13C2-6:2 FTS 95 50-150 1 06/20/2024 16:41 <br /> 13C2-8:2 FTS 91 50-150 1 06/20/2024 16:41 <br /> 13C2-PFDoA 102 50-150 1 06/20/2024 16:41 <br /> 13C2-PFTeDA 104 50-150 1 06/20/2024 16:41 <br /> 13C3-HFPO-DA 105 50-150 1 06/20/2024 16:41 <br /> 13C3-PFBS 105 50-150 1 06/20/2024 16:41 <br /> 13C3-PFHxS 105 50-150 1 06/20/2024 16:41 <br /> 13C4-PFBA 104 50-150 1 06/20/2024 16:41 <br /> 13C4-P F H pA 104 50-150 1 06/20/2024 16:41 <br /> 13C5-PFHxA 102 50-150 1 06/20/2024 16:41 <br /> 13C5-PFPeA 107 50-150 1 06/20/2024 16:41 <br /> 13C6-PFDA 103 50-150 1 06/20/2024 16:41 <br /> 13C7-PFUdA 104 50-150 1 06/20/2024 16:41 <br /> 13C8-PFDA 108 50-150 1 06/20/2024 16:41 <br /> 13C8-PFOS 104 50-150 1 06/20/2024 16:41 <br /> 13C8-PFOSA 99 50-150 1 06/20/2024 16:41 <br /> 13C9-PFNA 102 50-150 1 06/20/2024 16:41 <br /> d3-McFOSAA 99 50-150 1 06/20/2024 16:41 <br /> d5-EtFOSAA 104 50-150 1 06/20/2024 16:41 <br /> 13C2-PFHxDA 74 50-150 1 06/20/2024 16:41 <br /> d3-McFOSA 94 50-150 1 06/20/2024 16:41 <br /> d5-EtFOSA 97 50-150 1 06/20/2024 16:41 <br /> d7N-McFOSE 96 50-150 1 06/20/2024 16:41 <br /> d9N-EtFOSE 87 50-150 1 06/20/2024 16:41 <br /> Analyst(s): STA <br /> (Cont.) <br /> DoD-ELAP Cert#L22-757•CA ELAP 1644 <br /> Page 15 of 30 <br />