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Alpha Analytical Laboratories, Inc. email: rlientservices alpha-labs.com Corporate: 208 Mason Street I Ukiah, CA 95482 1 T, 707468-C401 l R 707468-5267 1 EL.AP# 1551 McCampbell Analytical/Alpha Quote 232557 Project Manager: Lab Reports 1534 Willow Pass Rd. Project: Soil Testing Reported: Pittsburg, CA 94565 Project Number: LLNL 13882-Disp 10/14/25 12:59 Volatile Organic Compounds by EPA Method 8260B-Quality Control Reporting Spike Source %REC RPD Analyte(s) Result Limit Units Level Result %REC Limits RPD Limit Flag Batch AJ53925-NB EPA 5030 Soil GCMS MRL Check(AJ53925-MRLl) Prepared&Analyzed: 10/10/25 1,1-Dichloroethane 3.55 2.5 ug/kg 2.50 142 50-200 Di-isopropyl ether 2.58 2.5 ug/kg 2.50 103 50-200 cis-1,2-Dichloroethene 3.08 2.5 ug/kg 2.50 123 50-200 2,2-Dichloropropane 3.40 2.5 ug/kg 2.50 136 50-200 Chloroform 3.48 2.5 ug/kg 2.50 139 50-200 Bromochloromethane 3.50 2.5 ug/kg 2.50 140 50-200 Tetrahydrofuran 3.25 2.5 ug/kg 2.50 130 50-200 1,1,1-Trichloroethane 3.38 2.5 ug/kg 2.50 135 50-200 1,2-Dichloroethane 3.55 2.5 ug/kg 2.50 142 50-200 1,1-Dichloropropene 2.68 2.5 ug/kg 2.50 107 50-200 Carbon tetrachloride 3.32 2.5 ug/kg 2.50 133 50-200 Benzene 3.30 2.5 ug/kg 2.50 132 50-200 Tert-amyl methyl ether 2.35 2.5 ug/kg 2.50 94.0 50-200 Trichloroethene 3.15 2.5 ug/kg 2.50 126 50-200 1,2-Dichloropropane 3.25 2.5 ug/kg 2.50 130 50-200 Dibromomethane 3.45 2.5 ug/kg 2.50 138 50-200 Bromodichloromethane 3.22 2.5 ug/kg 2.50 129 50-200 cis-1,3-Dichloropropene 2.38 2.5 ug/kg 2.50 95.0 50-200 Toluene 3.40 2.5 ug/kg 2.50 136 50-200 trans-1,3-Dichloropropene 2.58 2.5 ug/kg 2.50 103 50-200 1,1,2-Trichloroethane 3.30 2.5 ug/kg 2.50 132 50-200 1,3-Dichloropropane 2.92 2.5 ug/kg 2.50 117 50-200 Dibromochloromethane 2.80 2.5 ug/kg 2.50 112 50-200 Tetrachloroethene 2.98 2.5 ug/kg 2.50 119 50-200 1,2-Dibromoethane(EDB) 2.98 2.5 ug/kg 2.50 119 50-200 Chlorobenzene 3.48 2.5 ug/kg 2.50 139 50-200 1,1,1,2-Tetrachloroethane 3.05 2.5 ug/kg 2.50 122 50-200 Ethylbenzene 2.62 2.5 ug/kg 2.50 105 50-200 m,p-Xylene 4.90 5.0 ug/kg 5.00 98.0 50-200 o-Xylene 2.32 2.5 ug/kg 2.50 93.0 50-200 Styrene 2.15 2.5 ug/kg 2.50 86.0 50-200 Xylenes(total) 7.22 7.5 ug/kg 7.50 96.3 50-200 Bromoform 2.88 2.5 ug/kg 2.50 115 50-200 1,1,2,2-Tetrachloroethane 3.08 2.5 ug/kg 2.50 123 50-200 Isopropylbenzene 2.02 2.5 ug/kg 2.50 81.0 50-200 The results in this report apply to the samples analyzed in accordance with the chain of custody document.This analytical report must be reproduced in its entirety. Page 11 of 18