Laserfiche WebLink
TO E RO E K SOP No.021,REV.1 <br /> „ SOIL GAS SAMPLING METHODS <br /> ASSOCIATES,INC. <br /> PAGE 6 <br /> or equivalent sampling tube. To prevent ambient air from entering the canister during sample <br /> collection, all connections must be airtight. To collect soil gas samples using this method, the <br /> following procedures are used: <br /> 1. Confirm the valve is closed and remove the brass cap. Attach the pressure gauge and flow <br /> controller(integrated system)to the canister. Attach the soil probe to the sample train with <br /> Tygon or equivalent tubing. <br /> 2. Open the canister valve, which will allow the evacuated canister to draw in soil gas, and <br /> immediately record the canister pressure reading and time. <br /> 3. Monitor sampling progress periodically. When target sample collection time has been <br /> reached, close the canister valve. <br /> 4. Record the time and post-sampling pressure reading on the canister pressure valve. Do not <br /> let the vacuum be reduced to zero pressure as this will compromise the analytic results. <br /> 5. Remove the canister from the sample train and replace the brass cap. <br /> 6. Follow the leak check procedures described in Section 2.8. <br /> 7. Label the canister and its corresponding field data sheet with the sample number. <br /> 8. Fill out the rest of the field data sheet and chain of custody and document all information <br /> in a field logbook. <br /> 9. Ship samples to the laboratory for analysis. Summa samples do not need to be chilled after <br /> collection or during transportation. <br /> 2.6 SAMPLE COLLECTION USING SORBENT TUBES <br /> Sorbent tubes are provided by the laboratory, and selection of the sorbent tube media is dependent <br /> on the compounds to be reported. The pump should be calibrated before sample collection begins, <br /> and flow rates should be recorded. To collect soil gas samples using this method, the following <br /> procedure is used: <br /> 1. Connect the sampling inlet end of the sorbent tube to the soil gas probe with a union fitting. <br /> 2. Connect the other end of the sorbent tube to the pump using Tygon® or equivalent tubing. <br /> 3. Start the pump and record the start time. After the desired duration, stop the pump and <br /> record the end time. <br /> 4. Remove the sorbent tube from the probe and pump, and replace the end plugs on both ends <br /> of the tube. <br /> 5. Follow the leak check procedures described in Section 2.8. <br /> 6. Record the sample number,tube number, sample flow rate, collection date and time on the <br /> field data sheet and chain of custody and document all information in a field logbook. <br /> 7. Due to the sampling medium, samples must be stored and transported in a cooler with ice <br />