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COLUMBIA ANALYTICAL SERVICES, INC <br /> Analytical Report <br /> . Client EMCON Service Request 59900683 <br /> Protect Apache Plastics/22640-100 001 Date Collected 2/24/99 <br /> Sample Mati ix Soil DAtL Received 3/2/99 <br /> Fuel Oxygenates <br /> Sample Name S 1 P-1234 Units ug/Kg(ppb) <br /> Lab Code 59900683-005 <br /> Test Notes Basis Wet <br /> Prep AnAysis Dilution Date Date Result <br /> Analyte Method Method MRI, Factor Extracted Analyzed Result Notes <br /> tent-Butyl Alcohol NONE 8260 500 1 3/4/99 3/9/99 ND <br /> Methyl tert-Butyl Lthe, NONE 8260 5 1 3/4/99 3/9/99 ND <br /> Diisopropyl Ether NONE 8260 50 1 3/4/99 3/9/99 ND <br /> Ethyl tent-Butyl Ether NONE 8260 50 1 3/4/99 3/9/99 ND <br /> tent-Amyl Methyl Ether NONE 8260 50 1 3/4/99 3/9/99 ND <br /> Ethanol NONE 8260 5000 1 3/4/99 3/9/99 ND <br /> • <br /> Isaa021197p <br /> Page 3 <br />