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COLUMBIA ANALYTICAL SERVICES, INC <br /> Analytical Report <br /> I <br /> Client EMCON Service Request 59900683 <br /> Protect Apd(,he Plastics/22640-100 001 Date Collected 2/23/99 <br /> Sample Matrix Soil Date Received 3/2/99 <br /> Fuel Oxygenates <br /> Sample Name B-1(66) Units ug/Kg(ppb) <br /> Lab Code 59900683-006 Basis Wet <br /> Test Notes <br /> Prep Analysis Dilution Date Date Result <br /> Analyte Method Method MRL Factor Extracted Analyzed Result Notes <br /> tert-Butyl Alcohol NONE 8260 500 1 3/4/99 3/4/99 ND <br /> Methyl tert-Butyl Ether NONE 8260 5 1 3/4/99 3/4/99 ND <br /> Diisopropyl Ether NONE 8260 50 l 3/4/99 3/4/99 ND <br /> Ethyl tert-Butyl Ether NONE 8260 50 1 3/4/99 3/4/99 ND <br /> tert-Amyl Methyl Ether NONE 8260 50 1 3/4/99 3/4/99 ND <br /> Ethanol NONE 8260 5000 1 3/4/99 3/4/99 ND <br /> I <br /> I <br /> IS44/D21-497p <br /> Page 4 <br />