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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Report <br /> Client- EMCON Service Request 59900683 <br /> Project Apache 1`14stics/22640-100 001 Date Collected 2/22/99 <br /> Sample Mat,Ia Soil Date Received 3/2/99 <br /> Fuel Oxygenates <br /> Sample Name B-2(82) Units ug/Kg(ppb) <br /> Lab Code 59900683-010 Basis Wet <br /> Test Notes <br /> Piep Analysis Dilution Datc Date Result <br /> Analyte Method Method MRL Factor Extracted Analyzed Result Notes <br /> tett-Butyl Alcohol NONE 8260 500 1 3/4199 3/4/99 ND <br /> Methyl tent-Butyl Ethel NONE 8260 5 1 314199 3/4/99 ND <br /> Dusopropyl Ether NONE 8260 50 1 3/4/99 3/4/99 ND <br /> Ethyl tert-Butyl Ether NONE 8260 50 1 3/4199 3/4/99 ND <br /> lei t-Amyl Methyl Ether NONE 8260 50 1 3/4199 3/4/99 ND <br /> Ethanol NONE 8260 5000 1 3/4/99 3/4/99 ND <br /> 15441921197p <br /> Page 8 <br />