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COLUMBIA ANALYTICAL SERVICES, INC <br /> Analytical Report <br /> Client EMCON Service Request S9900693 <br /> Project AP LLhe Pldstic,/22640-100 001 Date Collected 2/22/99 <br /> Sample Matz ix Sol] Date Received 3/2/99 <br /> Fuel Oxygenates <br /> Sample Name B-2(96) Units ug/Kg(ppb) <br /> Lab Code 59900683-011 Basis Wet <br /> Test Notes <br /> Prep Analysis Dilution Date Date Result <br /> Analyte Method Method MRL Factor Extracted Analyzed Result Notes <br /> tent-Butyl Alcohol NONE 8260 500 1 3/4/99 3/4/49 ND <br /> Methyl Cert-Butyl Ether NONE 8260 5 ] 3/4/99 3/4/99 ND <br /> Dilsopropyl Ether NONE 8260 50 1 314199 3/4/99 ND <br /> Ethyl tent-Butyl Ether NONE 8260 50 1 314/99 3/4/99 ND <br /> Cert-Amyl Methyl Ether NONE 8260 50 ] 3/4/99 3/4/99 ND <br /> Ethanol NONE 8260 5000 1 3/4/99 3/4/99 ND <br /> 15441021-497p <br /> Page 9 <br />