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f <br />AlLancaster <br />Laboratories <br />*- Outside of specification <br />F(1) The result for one or both determinations was less than five times the LOQ, <br />(--12) The background result was more than four times the spike added. <br />Lancaster Laboratories, Inc. <br />M E M B E R 2425 New Holland Pike <br />FICBax 12425 <br />La <br />� Lancaster, PA 17605-2425 <br />777-656-2300 Fax: 717-656-2697 <br />DLYP <br />RPD <br />Page 3 of 4 <br />Dup <br />RPD <br />Max <br />Quality <br />Control Summary <br />Client Name: ChevronTexaco <br />Reported: 11/07/03 at 10:50 AM <br />Group Number: 872526 <br />Sample Matrix <br />Quality Control <br />MS <br />MSD MS/MSD <br />RPD Bite Di7P <br />Anal ais Name %REC <br />t -Amyl methyl ether <br />. %REC Limits <br />RPD MAX Conc Conc <br />t -Butyl alcohol 96 <br />104 <br />77-117 <br />0 30 <br />Benzene <br />10 <br />104 44-150 <br />0 30 <br />1,2-Dichloroethane 101 <br />101 83-128 <br />1 30 <br />Toluene 96 <br />99 <br />97 73-136 <br />100 83-127 <br />1 30 <br />1,2-Dibromoethane <br />1 30 <br />Ethylbenzene 93 <br />94 78-120 <br />1 30 <br />102 <br />Xylene (Total) <br />103 82-129 <br />1 30 <br />100 <br />102 82-130 <br />2 30 <br />Surrogate <br />Quality Control <br />Analysis Name: TPH-GRO - Waters <br />Batch number: 03302A55A <br />rv� TriFluorotoluene-F <br />F <br />9152395 79 <br />a` 4152396 74 <br />4152397 74 <br />152398 74 <br />4152399 75 <br />Blank 75 <br />LCS 82 <br />LCSD 76 <br />Ms 80 <br />Limits: 57-146 <br />Analysis Name: Methanol and Ethanol <br />Batch number: 033070007A <br />Acetone <br />4152395 log <br />4152396 106 <br />4152397 103 <br />4152398 109 <br />4152399 106 <br />Blank 103 <br />LCS 104 <br />MS 99 <br />MSD 102 <br />Limits: 72-128 <br />Analysis Name: BTEX+5 Oxygenates+EDC+EDB+ETOH <br />*- Outside of specification <br />F(1) The result for one or both determinations was less than five times the LOQ, <br />(--12) The background result was more than four times the spike added. <br />Lancaster Laboratories, Inc. <br />M E M B E R 2425 New Holland Pike <br />FICBax 12425 <br />La <br />� Lancaster, PA 17605-2425 <br />777-656-2300 Fax: 717-656-2697 <br />DLYP <br />RPD <br />Page 3 of 4 <br />Dup <br />RPD <br />Max <br />