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r <br />AIPLancaster <br />Laboratories <br />Quality Control Summary <br />Client Name: ChevronTexaco <br />Reported: 11/07/03 at 10:50 AM Croup Number: 872526 <br />Su <br />Page 4 of 4 <br />*- Outside of specification <br />1) The result for one or both determinations was less than five times the LOQ. <br />f� (2) The background result was more than four times the spike added. <br />LancasterLaboratories, Inc, <br />M E M B E R 2425 New Holland Pike <br />PO Box 12425 <br />Lancaster, PA 17605-2425 <br />717-656-?3DO F..: 717-656-2681 <br />ti 116 nr, ., R�1 N(53 <br />Batch number: P033021AA <br />rrogate <br />Quality Control <br />Dibromofluoromethane <br />1,2-Dichloroethane-d4 <br />4152395 <br />Toluene -d8 <br />4--gromofluozobenzene <br />101 <br />95 <br />Blank <br />100 <br />96 <br />101 <br />99 <br />LCS <br />101 <br />96 <br />101 <br />98 <br />Ms <br />101 <br />gq <br />103 <br />100 <br />MSD <br />102 <br />94 <br />103 <br />106 <br />102 <br />105 <br />Limits: <br />81-120 <br />82-112 <br />B5-li2 <br />83-113 <br />Analysis <br />Name: STEX+5 Oxygenates+EDC+EDB+ETON <br />Batch number: P033023AA <br />Dibromofluoromethane <br />1,2-Dichloroethane-d4 <br />Toluene -d8 <br />4-Bromofluorobenzene <br />4152396 <br />101 <br />95 <br />4152397 <br />101 <br />94 <br />102 <br />98 <br />4152398 <br />101 <br />96 <br />102 <br />99 <br />Blank <br />101 <br />955 <br />101 <br />98 <br />LCS <br />101 <br />96 <br />101 <br />99 <br />MS <br />100 <br />102 <br />104 <br />MSD <br />102 <br />97 <br />101 <br />101 <br />� <br />101 <br />99 <br />Limits: <br />81-120 <br />B2-112 <br />85-112 <br />83 113 <br />Analysis <br />Name: STEX+5 Oxygenates+EDC+EDB+ETOH <br />Batch number: P033031AA <br />Dibromofluoromethane <br />1,2-Dichloroethane-d4 <br />Toluene -d8 <br />4-Bromofluorobenzene <br />4152399 <br />102 <br />97 <br />Blank <br />142 <br />101 <br />99 <br />LCS <br />102 <br />995 <br />101 <br />99 <br />Ms <br />102 <br />97 <br />101 <br />100 <br />MSD <br />102 <br />100 <br />9996 <br />101 <br />140 <br />Limits: <br />81-120 <br />82-112 <br />1. <br />85-112 <br />83-113 <br />*- Outside of specification <br />1) The result for one or both determinations was less than five times the LOQ. <br />f� (2) The background result was more than four times the spike added. <br />LancasterLaboratories, Inc, <br />M E M B E R 2425 New Holland Pike <br />PO Box 12425 <br />Lancaster, PA 17605-2425 <br />717-656-?3DO F..: 717-656-2681 <br />ti 116 nr, ., R�1 N(53 <br />