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Lancaster <br />Laboratories Analysis Report <br />2425 New Hof)and pike, PO Box 12425, Lancasler, PA 17605-2425 •717-656-2300 Fax:717-656-2681 • www.lancastoriabs.com <br />Page i of 2 , <br />Quality Control Summary 15 <br />Client Name: ChevronTexaco Group Number: 894553 <br />Reported: 05/14/04 at 05:37 PM <br />Matrix QC may not be reported if site-specif c QC samples were not � <br />submitted, In these situations, to demonstrate precision and accuracy at <br />a batch level, a LCS/LCSD was performed, unless otherwise specified in the <br />method. <br />*- Outside of specification <br />(l ) The result for one or both determinations was less than five times the LOQ. <br />(2) The background result was more than four times the spike added. <br />Laboratory Compliance Quality <br />Control <br />Analysis Name <br />Blank <br />Result <br />Blank Report <br />HL <br />LC8 <br />LC8D <br />LC6/LCSD <br />Units <br />ABC <br />IRKC- <br />Limits <br />UD RPD Marc <br />Batch number: 04127A07E <br />TPH-GRO <br />Sample <br />number (13). 4266325 <br />- Waters <br />N.D. <br />50. ug/l <br />86 <br />86 <br />70-130 <br />1 30 <br />Batch number; 041310024A <br />Methanol (by Direct Injection) <br />Sample <br />N.D. <br />number(s): 4266325 <br />200, ug/l <br />92 <br />76-119 <br />Hatch number: P041331AA <br />Ethanol <br />Sample <br />number(s). 4266325 <br />Methyl Tertiary Butyl Ether <br />N.D. <br />N.D. <br />50. u9/1 <br />0.5 ug/i <br />97 <br />98 <br />46-145 <br />di -Isopropyl ether <br />N.D. <br />0.5 ug/l <br />92 <br />77-127 <br />Ethyl t -butyl ether <br />N.D. <br />0.5 ug/l <br />92 <br />67-130 <br />74-120 <br />t -Amyl methyl ether <br />t -Butyl alcohol <br />N.D. <br />0.5 u§/1 <br />101 <br />79-113 <br />j <br />Benzene <br />N.D. <br />N.D. <br />5. ug/l <br />0.5 ug/l <br />109 <br />99 <br />57-141 <br />1.2-Dichloroethane <br />N.D. <br />0.5 ug/1 <br />92 <br />85-117 <br />Toluene <br />1,2-Dibromoethane <br />N.D. <br />0.5 ug/l <br />95 <br />77-132 <br />85-115 <br />8thylbenzene <br />N.D. <br />N.D. <br />. <br />05 u 1 <br />0.5 ug/l <br />95 <br />93 <br />81-114 <br />i <br />Xylene (Total) <br />N.D. <br />0.5 ug/l <br />96 <br />82-119 <br />84-120 <br />Sample Matrix <br />Quality <br />Control <br />Anslynia, Name <br />--- <br />M& <br />IREC <br />MSD MS/MSD <br />%RSC Limits RPD1k1 <br />RPD <br />SKG <br />DUP <br />DUP Dup RPD <br />Conc <br />Cork <br />RD Nam ,..i <br />Batch number: 04127A07E <br />Sample <br />number(s); 4266325 <br />TPH-GRO - Waters <br />89 <br />63-154 <br />i <br />Batch number; 041310024A <br />Sample <br />number(s)- 4266325 <br />Methanol (by Direct Injection) <br />96 <br />96 72-122 0 <br />20 <br />Batch. number: P041331AA <br />Sample <br />number(s): 4266325 <br />t <br />j <br />Ethanol <br />Methyl Tertiary Butyl Ether <br />99 <br />102 <br />80 41-155 21 <br />94 69-134 8 <br />30 <br />di -Isopropyl ether <br />97 <br />89 75-130 8 <br />30 <br />30 <br />i <br />Ethyl t -butyl ether <br />95 <br />88 78-119 8 <br />30 <br />t -Amyl methyl ether <br />103 <br />94 77-117 9 <br />30 <br />t -Butyl alcohol <br />112 <br />100 51-147 12 <br />30 <br />Benzene <br />1,2-Dichloroethane <br />105 <br />96 <br />97 83-128 8 <br />87 <br />30 <br />Toluene <br />104 <br />73-136 9 <br />92 83-127 13 <br />30 <br />30 <br />1,2-Dibromoethane <br />100 <br />90 70-120 11 <br />30 <br />*- Outside of specification <br />(l ) The result for one or both determinations was less than five times the LOQ. <br />(2) The background result was more than four times the spike added. <br />