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Lancaster <br />Laboratories Analysis Report <br />2425 New Holland Pike, PO Box 12425, Lancaster. PA 17605-2425 •717-656-2300 F�ax;717-656.2681 • www.lancaslerlab5.con1 <br />Page 2 of 2 <br />4. Quality Control.Summary <br />Client Name: ChevronTexaco <br />Reported: 05/14/04 at 05:37 PM <br />Analysis Name <br />Ethylbenzene <br />Xylene (Total) <br />Group Number: 894553 <br />Sample Matrix Quality Control <br />MS NSD MS/MSD RPD BRQ DUP <br />%REP $kPEC Limits RPD l;rA]I Conc cony <br />101 91 82-129 11 30 <br />104 94 82-130 10 30 <br />Surrogate Quality Control <br />Analysis Name-- TPH-GRO - Platers <br />Batch number: 04127A07E <br />Trifluorotoluene-F <br />Blank 86 <br />LCS 104 <br />LCSD 104 <br />MS 104 <br />?Analysis Name: Methanol and Ethanol <br />Batch number: 041310024A <br />Acetone <br />4266325 99 <br />Blank 94 <br />LCS 94 <br />MS 95 <br />MSD 94 <br />DUP Dup RPA <br />RPD MAX <br />*- Outside of specification <br />(1) The result for one or both determinations was less than five times the LOQ. <br />(2) The background result was more than four times the spike added. <br />F. <br />r <br />Limits: <br />80-132 <br />Analysis <br />Name: BTEX+5 oxygenates+EDC+EDB+ETON <br />Batch number: P041331AA <br />Dibromofluoromethane 1,2-Dichl6roethane-d4 <br />Toluene -d8 <br />,4-Bromofluorobenzene <br />4266325 <br />101 94 <br />95 <br />94 <br />Blank <br />101 94 <br />94 <br />93 <br />LCS <br />100 95 <br />95 <br />93 <br />MS <br />100 94 <br />96 <br />96 <br />MSD <br />loo 95 <br />95 <br />94 <br />Limits: <br />81-120 82-112 <br />85-112 <br />83-113 <br />*- Outside of specification <br />(1) The result for one or both determinations was less than five times the LOQ. <br />(2) The background result was more than four times the spike added. <br />F. <br />r <br />