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1 <br />Lancaster <br />Laboratories <br />Quality Control Summary <br />1 Client Name ChevronTexaco <br />Reported 04/03/03 at 10 50 AM <br />4016359 98 <br />4016360 97 <br />4016361 100 <br />Blank 103 <br />LCS 102 <br />MS 102 <br />MSD 101 <br />'Limits 72-128 <br />Analysis Name TPH-GRO - Waters <br />Batch number 03083A16A <br />Trifluorotoluene-F <br />' 49 112 <br />Limits 57-146 <br />Analysis Name TPH-GRO - Waters <br />Batch number 03083A51B <br />Trifluorotoluene-F <br />Group Number 845781 <br />Surrogate Quality Control <br />4 0 6 6 1 90 <br />4016361 90 <br />Blank 90 <br />LCS 93 <br />LCSD 94 <br />MS 90 <br />Limits 57-146 <br />'Analysis Name BTEX + Oxygenates by 8260E <br />Batch number P030852AA <br />Dlbromofluoromethane 1,2-Dichloroethane-d4 Toluene -d8 <br />Page 3 of 4 <br />4-Bromofluorobenzene <br />4016357 <br />108 <br />98 <br />99 <br />107 <br />'4016358 <br />4016359 <br />107 <br />100 <br />Blank <br />107 <br />LCS <br />112 <br />' 49 112 <br />Limits 57-146 <br />Analysis Name TPH-GRO - Waters <br />Batch number 03083A51B <br />Trifluorotoluene-F <br />Group Number 845781 <br />Surrogate Quality Control <br />4 0 6 6 1 90 <br />4016361 90 <br />Blank 90 <br />LCS 93 <br />LCSD 94 <br />MS 90 <br />Limits 57-146 <br />'Analysis Name BTEX + Oxygenates by 8260E <br />Batch number P030852AA <br />Dlbromofluoromethane 1,2-Dichloroethane-d4 Toluene -d8 <br />Page 3 of 4 <br />4-Bromofluorobenzene <br />'*- Outside of specification <br />1 The result for one or both determinations was less than five times the LOQ <br />The background result was more than four times the spike added <br />Lancaster Laboratories, Inc <br />99 <br />98 <br />99 <br />97 <br />'4016358 <br />4016359 <br />100 <br />100 <br />99 <br />98 <br />4016360 <br />99 <br />101 <br />99 <br />96 <br />4016361 <br />100 <br />103 <br />98 <br />97 <br />Blank <br />LCS <br />99 <br />101 <br />98 <br />96 <br />99 <br />99 <br />96 <br />97 <br />MS <br />99 <br />103 <br />99 <br />97 <br />'*- Outside of specification <br />1 The result for one or both determinations was less than five times the LOQ <br />The background result was more than four times the spike added <br />2216 Rev 1012/02 <br />Lancaster Laboratories, Inc <br />' M E M B E R <br />®PO <br />2425 New Holland Pike <br />Bax 12425 <br />Lancaster 17605 1 <br />717 656-230000 Fax 7177 656 2681 <br />2216 Rev 1012/02 <br />