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Lancaster <br />• Laboratories <br />Quality Control Summary <br />Client Name ChevronTexaco Group Number 845781 <br />Reported 04/03/03 at 10 50 AM <br />'Surrogate Quality Control <br />MSD 100 98 100 98 <br />Limits 81-120 82-112 85-112 83-113 <br />Analysis Name BTEX + Oxygenates by 8260E <br />Batch number P030862AA <br />Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene -d8 <br />Page 4 of 4 <br />4-Bromofluorobenzene <br />'4016357 <br />Blank <br />LCS <br />'MS <br />MSD <br />101 <br />100 <br />100 <br />99 <br />99 <br />101 <br />100 <br />97 <br />104 <br />101 <br />98 <br />99 <br />99 <br />99 <br />100 <br />95 <br />97 <br />97 <br />96 <br />96 <br />Limits <br />81-120 <br />82-112 <br />85-112 <br />83-113 <br />t <br />'*- Outside of specification <br />(1) The result for one or both determinations was less than five tunes the LOQ <br />OThe background result was more than four times the spike added <br />Lancaster Laboratories inc <br />' <br />MEMBER 2425 New Holland Pike <br />®PO Box 12425 <br />Lancaster 1760x <br />717 656 230D00 fax 71717 655-2681 <br />2216 Rev 1012102 <br />