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*- Outside of specification <br />The result for one or both determinations was'less than five times the LOQ. <br />The background result was more than four times the spike added. <br />Lancaster Laboratories, Inc. <br />MEMBER 2425 New Holland Pike <br />PO Box 12425 _ <br />Lancaster.PA 17605-2425 <br />717-fi56-230000 Fax: 717-656-2681 2216 Rev. 9l11/00 <br />Lancaster Laboratories <br />Page 7 of 8 <br />Why fjtti a j*ol Summary <br />Client Name: ChevronTexaco Group Number: 817247 <br />Reported: <br />08/15/02 at 03:42 PM <br />Surrogate Quality <br />Control <br />3869040 <br />97 <br />3869041 <br />98 <br />3669042 <br />99 <br />3869043 <br />97 <br />3669044 <br />99 <br />386904$ <br />112 <br />3869046 <br />101 <br />3869047 <br />97 <br />Blank <br />102 <br />LCS <br />100 <br />MS <br />94 <br />MSD <br />95 <br />Limits: <br />72-128 <br />Analysis Name: BTEC + Oxygenates by 6260B <br />Batch number: N022142AB <br />Dibromofluoromethane 1,2-Dichloroethane-d4 <br />Toluene -d8 <br />4-Bromofluorobenzene <br />3869019 <br />104 101 <br />102 <br />95 <br />3869020 <br />104 104 <br />100 <br />94 <br />3869021 <br />105 102 <br />101 <br />94 <br />Blank <br />103 103 <br />101 <br />95 <br />100 lea <br />104 <br />104 <br />49 <br />99 103 <br />104 <br />104 <br />100 101 <br />104 <br />103 <br />Limits: <br />86-118 80-120 <br />88-110 <br />86-115 <br />AnalysiB'Natne: BTEX + Oxygenates by 8260B <br />Batch number: P022121AB <br />Dibromofluoromethane 1,2-Dichloroethane-d4 <br />Toluene -d8 <br />4-Bromofluorobenzene <br />3869022 <br />96 96 <br />93 <br />88 <br />3869023 <br />96 95 <br />93 <br />87 <br />3869024 <br />96 96 <br />93 <br />87 <br />3869025 <br />96 96 <br />93 <br />88 <br />3869026 <br />97 97 <br />93 <br />87 <br />3869027 <br />96 96 <br />93 <br />88 <br />3869028 <br />96 97 <br />93 <br />.88 <br />Blank <br />94 95 <br />94 <br />89 <br />LCS <br />93 94 <br />95 <br />93 <br />MS <br />92 94 <br />96 <br />92' <br />MSD <br />93 95 <br />95 <br />92 <br />Limits: <br />86-118 80-120 <br />88-110 <br />86-115 <br />Analysis Name: BTEX + Oxygenates by 82608 <br />Batch number: P022121AC <br />.Dibromofluoromethane 1,2-Dichloroethane-d4 <br />Toluene -dB <br />4-Bromofluorobenzene <br />3869029 <br />96 96 <br />93 <br />88 <br />*- Outside of specification <br />The result for one or both determinations was'less than five times the LOQ. <br />The background result was more than four times the spike added. <br />Lancaster Laboratories, Inc. <br />MEMBER 2425 New Holland Pike <br />PO Box 12425 _ <br />Lancaster.PA 17605-2425 <br />717-fi56-230000 Fax: 717-656-2681 2216 Rev. 9l11/00 <br />