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*- Outside of specification <br />The result for one or both determinations was less than five times the LOQ. <br />The background result was more than four times the spike added. <br />Lancaster Laboratories, Inc. <br />M E M B E Fi 2425 New Holland Pike <br />PO Box 12425 <br />Lancaster, PA 17805-2425 <br />717.656.2300 Fax: 717-656-2681 2216 Rev. 9/11100 <br />Lancaster Laboratories <br />page 8 of8 <br />1,1 d Wha2xqiM11xyaz&nVro1 Summary <br />Client Name: <br />ChevronTexaco Group Number: 817247 <br />Reported: <br />08/15/02 at 03:42 PM <br />Surrogate Quality Control <br />3869030 <br />97 96 <br />93 <br />87 <br />3869031 <br />97 96 <br />93 <br />87 <br />3869032 <br />97 96 <br />93 <br />86 <br />3869033 <br />97 96 <br />93 <br />87 <br />Blank <br />96 96 <br />93 <br />8s <br />LCs <br />93 94 <br />95 <br />93 <br />Ms <br />92 94 <br />96 <br />92 <br />MSD <br />93 95 <br />95 <br />92 <br />Limits: <br />86-118 80-120 <br />86-110 <br />86-115 <br />Analysis Name: BTEX + Oxygenates by 8260E <br />Batch number: P022141AA <br />Dibromofluoromethane 1,2-Dichloroethane-d4 <br />Toluene-de <br />4-Bromofluorobenzene <br />3869034 <br />95 96 <br />94 <br />88 <br />3869035 <br />96 96 <br />95 <br />88 <br />3869036 <br />95 96 <br />95 <br />87 <br />3869037 <br />96 98 <br />95 <br />88 <br />3869038 <br />96 96 <br />95 <br />88 <br />3869039 <br />95 96 <br />95 <br />88 <br />3869040 <br />95 97 <br />95 <br />87 <br />3869041 <br />95 96 <br />94 <br />87 <br />69043 <br />97 94 <br />94 <br />88 <br />9044 <br />96 99 <br />95 <br />87 <br />69045 <br />96 96 <br />96 <br />88 <br />3869046 <br />96 96 <br />95 <br />88 <br />3869047 <br />96 97 <br />94 <br />87 <br />Blank <br />96 96 <br />93 <br />88 <br />LCS <br />94 96 <br />95 <br />92 <br />LCSD <br />94 96 <br />95 <br />91 <br />"S <br />94 97 <br />96 <br />91 <br />Limits: <br />86-116 80-120 <br />88-110 <br />86-115 <br />Analysis Name: BTEX + Oxygenates by 82608 <br />Batch number: P022141AB <br />Dibromofluoromethane 1,2-Dichloroethane-d4 <br />Toluene-d8 <br />4-Bromofluorobenzene <br />3669042 <br />98 97 <br />93 <br />87 <br />Blank <br />97 97 <br />95 <br />89 <br />LCs <br />94 96 <br />95 <br />92 <br />LcSFj <br />94 96 <br />95 <br />91 <br />MS <br />94 97 <br />96 <br />91 <br />Limits: <br />86-118 80-120 <br />88-110 <br />86-115 <br />*- Outside of specification <br />The result for one or both determinations was less than five times the LOQ. <br />The background result was more than four times the spike added. <br />Lancaster Laboratories, Inc. <br />M E M B E Fi 2425 New Holland Pike <br />PO Box 12425 <br />Lancaster, PA 17805-2425 <br />717.656.2300 Fax: 717-656-2681 2216 Rev. 9/11100 <br />