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Analytical Data <br /> Client Philips Environmental Services Corp Job Number 720-450-1 <br /> Client Sample ID SP-6 <br />' Lab Sample ID 720-450-13 Date Sampled 11/10/2005 1714 <br /> Client Matrix Water Date Received 11/11/2005 2015 <br /> 8260B Volatile Organic Compounds by GC/MS <br /> Method 8260B Analysis Batch 720-2007 Instrument ID Vanan 3900C <br /> Preparation 5030B Lab File ID c lsatumwsldata1200511111 <br />' Dilution 10 Initial WeightfVolume 10 mL <br /> Date Analyzed 11/16/2005 1406 Final Weight/Volume 10 mL <br /> Date Prepared 11/16/2005 1406 <br /> Analyte Result(ug/L) Qualifier RL <br /> 1,2-Dichloroethane ND 050 <br /> Benzene ND 0 50 <br /> Ethylbenzene ND 050 <br /> MTBE ND 050 <br /> TAME ND 050 <br />' Toluene ND 050 <br /> Xylenes,Total ND 10 <br /> TBA ND 50 <br /> DIPE ND 10 <br /> Gasoline Range Organics(GRO)-C5-C12 350 50 <br /> Ethyl tert-butyl ether ND 050 <br /> Surrogate %Rec Acceptance Limits <br /> Toluene-d8 102 77-121 <br /> 1,2-Dichloroethane-d4 112 73- 130 <br /> 1 <br /> r <br /> STL San Francisco Page 16 of 34 <br />