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Analytical Data <br />' Client Philips Environmental Services Corp Job Number 720-450-1 <br /> Client Sample ID PZ-1 <br />' Lab Sample ID 720-450-14 Date Sampled 11/10/2005 1610 <br /> Client Matrix Water Date Received 11/11/2005 2015 <br />' 82608 Volatile Organic Compounds by GC/MS <br /> Method 82608 Analysis Batch 720-2007 Instrument ID Varian 3900C <br /> Preparation 5030B Lab File ID c lsaturnwsldata1200511111 <br /> Dilution 10 Initial Weight/Volume 10 mL <br /> Date Analyzed 11/16/2005 1623 Final WeightlVolume 10 mL <br /> Date Prepared 11/16/2005 1623 <br />' Analyte Result(ug/L) Qualifier RL <br /> 1,2-Dichloroethane ND 50 <br /> ' Benzene 1100 5 0 <br /> Ethylbenzene 590 5 0 <br /> MTBE ND 5 0 <br /> TAME 18 5 0 <br /> ' Toluene 67 5 0 <br /> Xylenes,Total 1200 10 <br /> TBA ND- 50 <br /> DIPE 23 10 <br /> 10 Gasoline Range Organics(GRO)-C5-C12 9200 500 <br /> Ethyl tert-butyl ether ND 5 0 <br /> Surrogate %Rec Acceptance Limits <br /> Toluene-d8 105 77- 121 <br /> 1,2-Dichloroethane-d4 114 73- 130 <br /> 1 <br /> i <br /> STL San Francisco Page 17 of 34 <br />