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Inspection Report on hazardous waste manifest number 23440668 for treatment at Safety Kleen in Oakland. On or before February 10, 2005, Safety Kleen Oakland notified LLNL Site 300 that they could not accept the shipment of hazardous waste. On February 10, 2005, LLNL Site 300 picked up the rejected load of hazardous wastes at Safety Kleen in Oakland under new hazardous waste manifest number 23440682 and delivered the rejected load of hazardous waste to an alternate TSDF facility, Clean Harbors located in San Jose. Corrective Action: Within 7 days of receipt of this report, LLNL Site 300 shall comply with the. rejected load regulations specified in Health and Safety Code section 25160.6. 2- LLNL Site 300 violated Health and Safety Code section 25189 (a) in that on or about February 10, 2005, LLNL site 300 made, a false representation on hazardous waste manifest number 23440682. According to manifest number 23440682 on February 10, 2005, LLNL Site 300 released 7 containers of hazardous waste to LLNL as transporter to Clean Harbor of San Jose. Based on LLNL Site 300 documents and manifest 2340668, these same 7 containers were transported by Safety Kleen to Safety Kleen of Oakland on January 31, 2005. Upon arrival, the 7 containers of hazardous waste to Safety Kleen Oakland rejected the 7 containers. The 7 containers remained at Safety Kleen Oakland from January 31, 2005 until picked up for transporter by LLNL on February 10, 2005. Corrective Action: Within 7 days of receipt of this report, LLNL Site 300 shall comply with the rejected load regulations specified in Health and Safety Code section 25160.6. Unresolved issues since October 28, and 29, 2003, Compliance Evaluation Inspection (CEI) LLNL Site 300 violated California Code of Regulations, title 22, section 66264.16 in that on or before October 28, 2003, the facility failed to have a training plan as part of the Part B, Operating Plan for the post -closure unit Building 829. The facility response to the violation is currently under review by the Department. VII. Discussions with Operator: June 21, 2005: On June 21, 2005, after completing my inspection, I held an exit meeting with the facility representatives. I issued Summary of Observation (SOO). The SOO was signed by Ms. Folks. See attachment N I also discussed observations I made during the inspection with the facility representatives. I did identify an issue pertaining hazardous waste manifest number 23440668. The hazardous waste manifest showed that LLNL S 300 shipped seven containers of Non-RCRA hazardous waste, liquid (ethoxylted alcohols, trimethylhexanoic acid (MPC) on Page 18 of 20