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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3 Job Number: C35685 Account: DECASM Dysert Environmental Project: Pactiv Packaging- 1110 Performance Drive Stockton CA 95206 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch C35719-5MS M48875.D 1 08/31/14 TN n/a n/a VM1482 C35719-5MSD M48876.D 1 08/31/14 TN n/a n/a VM1482 C35719-5 M48861.D 1 08/31/14 TN n/a n/a VM1482 m A The QC reported here applies to the following samples: Method: SW846 8260B C35685-1 C35719-5 Spike MS MS Spike MSD MSD Limits CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg ug/kg % RPD Rec/RPD 67-64-1 Acetone NO 160 323 202*a 160 312 195*a 3 62-130/24 71-43-2 Benzene ND 40 35.2 88 40 34.6 87 2 81-119/20 108-86-1 Bromobenzene ND 40 30.6 77*a 40 30.1 75* a 2 79-120/22 74-97-5 Bromochloromethane ND 40 36.2 91 40 34.8 87 4 81-120/19 75-27-4 Bromodichloromethane ND 40 34.5 86 40 33.7 84 2 79-124/20 75-25-2 Bromoform ND 40 37.6 94 40 35.8 90 5 76-128/21 104-51-8 n-Butylbenzene ND 40 26.4 66*a 40 28.7 72*a 8 79-123/26 135-98-8 sec-Butylbenzene NO 40 31.4 79 40 33.4 84 6 77-122/24 98-06-6 Cert-Butylbenzene NO 40 34.5 86 40 35.8 90 4 77-121/23 108-90-7 Chlorobenzene ND 40 33.3 83 40 33.1 83 1 82-121/20 75-00-3 Chloroethane NO 40 29.8 75*a 40 29.3 73* a 2 80-126/21 67-66-3 Chloroform ND 40 35.0 88 40 34.1 85 3 82-123/20 95-49-8 o-Chlorotoluene ND 40 32.5 81 40 31.9 80 2 78-125/25 106-43-4 p-Chlorotoluene ND 40 28.1 70* a 40 29.8 75 6 75-125/26 56-23-5 Carbon tetrachloride ND 40 37.8 95 40 37.2 93 2 82-127/22 75-34-3 1,1-Dichloroethane ND 40 34.3 86 40 32.8 82 4 80-123/20 75-35-4 1,1-Dichloroethylene ND 40 36.7 92 40 35.1 88 4 76-123/19 563-58-6 1,1-Dichloropropene NO 40 37.8 95 40 36.9 92 2 79-123/20 96-12-8 1,2-Dibromo-3-chloropropane NO 40 34.7 87 40 33.5 84 4 64-133/23 106-93-4 1,2-Dibromoethane ND 40 35.6 89 40 34.6 87 3 80-120/20 107-06-2 1,2-Dichloroethane ND 40 35.5 89 40 33.9 85 5 76-132/21 78-87-5 1,2-Dichloropropane ND 40 34.4 86 40 33.5 84 3 80-121/20 142-28-9 1,3-Dichloropropane ND 40 33.9 85 40 33.1 83 2 78-120/20 108-20-3 Di-Isopropyl ether ND 40 30.8 77*a 40 29.7 74*a 4 78-126/19 594-20-7 2,2-Dichloropropane NO 40 35.0 88 40 34.3 86 2 77-132/22 124-48-1 Dibromochloromethane ND 40 35.6 89 40 34.7 87 3 76-121/21 75-71-8 Dichlorodifluoromethane ND 40 29.2 73 40 27.6 69 6 51-135/23 156-59-2 cls-1,2-Dichloroethylene ND 40 35.3 88 40 34.3 86 3 79-123/20 10061-01-5 cis-1,3-Dichloropropene ND 40 34.4 86 40 33.8 85 2 81-124/21 541-73-1 m-Dichlorobenzene ND 40 28.3 71*a 40 28.6 72*a 1 79-123/23 95-50-1 o-Dichlorobenzene ND 40 28.3 71*a 40 28.1 70*a 1 79-124/22 106-46-7 p-Dichlorobenzene NO 40 26.7 67*a 40 26.7 67*a 0 79-123/22 156-60-5 trans-1,2-Dichloroethylene ND 40 35.0 88 40 34.0 85 3 78-120/19 10061-02-6 Vans-1,3-Dichloropropene NO 40 32.1 80* a 40 30.7 77* a 4 81-123/22 100-41-4 Ethylbenzene ND 40 34.1 85 40 34.2 86 0 80-119/21 637-92-3 Ethyl tert-Butyl Ether ND 40 34.7 87 40 33.7 84 3 75-132/21 * = Outside of Control Limits. sib 30 of 64 v ACCUTE8T° C85685